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Technology Process of C6H5NNbCl(P(C6H5)(CH2Si(CH3)2N(C6H5))2)

C6H5NNbCl(P(C6H5)(CH2Si(CH3)2N(C6H5))2)

Base Information
  • Chemical Name:C6H5NNbCl(P(C6H5)(CH2Si(CH3)2N(C6H5))2)
  • CAS No.:623114-51-2
  • Molecular Formula:C30H36ClN3NbPSi2
  • Molecular Weight:654.14
  • Hs Code.:
C<sub>6</sub>H<sub>5</sub>NNbCl(P(C<sub>6</sub>H<sub>5</sub>)(CH<sub>2</sub>Si(CH<sub>3</sub>)2N(C<sub>6</sub>H<sub>5</sub>))2)

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Chemical Property of C6H5NNbCl(P(C6H5)(CH2Si(CH3)2N(C6H5))2)
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Technology Process of C6H5NNbCl(P(C6H5)(CH2Si(CH3)2N(C6H5))2)

There total 1 articles about C6H5NNbCl(P(C6H5)(CH2Si(CH3)2N(C6H5))2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nb(Cl)2(P(C<sub>6</sub>H<sub>5</sub>)(CH<sub>2</sub>Si(CH<sub>3</sub>)2N(C<sub>6</sub>H<sub>5</sub>))2)
623114-49-8

Nb(Cl)2(P(C6H5)(CH2Si(CH3)2N(C6H5))2)

C<sub>6</sub>H<sub>5</sub>NNbCl(P(C<sub>6</sub>H<sub>5</sub>)(CH<sub>2</sub>Si(CH<sub>3</sub>)2N(C<sub>6</sub>H<sub>5</sub>))2)
623114-51-2

C6H5NNbCl(P(C6H5)(CH2Si(CH3)2N(C6H5))2)

Guidance literature:
With KC8; In diethyl ether; High Pressure; addn. of ether to a flask contg. KC8 and Nb complex at -78°C, cooling with liquid N2 (-196°C), filling with 1 atm of N2, sealing, warming to room temp. within 2 h; evapn. to dryness, extn. into toluene, filtration, pptn. by addn. of hexanes;
DOI:10.1016/S0020-1693(02)01499-8
upstream raw materials:

Nb(Cl)2(P(C6H5)(CH2Si(CH3)2N(C6H5))2)

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