diphenatotris(pyridine)copper(II)

Base Information

• Chemical Name: diphenatotris(pyridine)copper(II)
• CAS No.: 89172-32-7
• Molecular Formula: C₂₉H₂₃CuN₃O₄
• Molecular Weight: 541.065

Synonyms:

Chemical Property of diphenatotris(pyridine)copper(II)

Chemical Property:

Purity/Quality:

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Technology Process of diphenatotris(pyridine)copper(II)

There total 1 articles about diphenatotris(pyridine)copper(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenatobis(pyridine)dicopper(I) + 9,10-phenanthrenequinone (84-11-7) + copper dichloride → dichloro(diphenato)tetrakis(pyridine)dicopper(II) (82762-12-7,76994-01-9) + diphenatotris(pyridine)copper(II) (89172-32-7)

Guidance literature:

With pyridine; oxygen; In pyridine; to CuCl2 in C5H5N saturated with O2 9,10-phenanthrenequinone and complex were added, mixt. was stirred under O2 for 5 h; crystals were filtered off, washed with ether, dried in vac., products were not separated;

DOI:10.1039/DT9830001995

Reference yield: 100.0%

diphenatotris(pyridine)copper(II) (89172-32-7) + copper (12775-96-1,15158-11-9,15721-63-8,16941-75-6,17493-86-6,19498-52-3,20499-83-6,20499-84-7,20499-85-8,20499-86-9,20573-10-8,20573-11-9,21595-51-7,21595-52-8,22206-52-6,26445-28-3,28959-95-7,37362-93-9,39417-05-5,54603-16-6,54603-23-5,54603-32-6,54603-40-6,54603-48-4,54603-81-5,54603-89-3,56316-56-4,95985-91-4,122297-32-9,7440-50-8) → diphenatobis(pyridine)dicopper(I)

Guidance literature:

In pyridine; complex and Cu in C5H5N were refluxed under Ar for 1 h; mixt. was filtered, filtrate was concd. in vac., residue was treated with ether for 2 h, compound was filtered off, washed with ether, dried invac.; elem. anal.;

DOI:10.1039/DT9830001995

upstream raw materials:

9,10-phenanthrenequinone

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