Fe(C₅H₅)(C₅H₃)CHCH₃OHP(C₆H₅)2

Base Information

• Chemical Name: Fe(C₅H₅)(C₅H₃)CHCH₃OHP(C₆H₅)2
• CAS No.: 74286-12-7
• Molecular Formula: C₂₄H₂₃FeOP
• Molecular Weight: 414.267
• Mol file: 74286-12-7.mol

Synonyms:

Chemical Property of Fe(C₅H₅)(C₅H₃)CHCH₃OHP(C₆H₅)2

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Fe(C₅H₅)(C₅H₃)CHCH₃OHP(C₆H₅)2

There total 1 articles about Fe(C₅H₅)(C₅H₃)CHCH₃OHP(C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(ScRp)-PPFOAc (74311-58-3,83378-24-9,74286-35-4) → Fe(C5H5)(C5H3)CHCH3OHP(C6H5)2 (74286-12-7,1006730-12-6,902525-82-0,277306-51-1)

Guidance literature:

With n-butyllithium; In diethyl ether; 1 h; water was added and the ether layer was sepd., washed with water and dried over K2CO3, the solvent was removed; elem. anal.;

DOI:10.1139/v82-246

Reference yield: 95.0%

[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) + Fe(C5H5)(C5H3)CHCH3OHP(C6H5)2 (74286-12-7,1006730-12-6,902525-82-0,277306-51-1) → [RuH(p-cymene){C5H3(PPh2)(CMeO)}]

Guidance literature:

In methanol; at 0 ℃; for 2h; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1002/ejic.201601440

Reference yield: 73.0%

[(η6-benzene)RuCl2(acetonitrile)] (154790-97-3) + Fe(C5H5)(C5H3)CHCH3OHP(C6H5)2 (74286-12-7,1006730-12-6,902525-82-0,277306-51-1) → [RuH(C6H6){C5H3(PPh2)(CMeO)}]

Guidance literature:

In methanol; for 1.2h; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1002/ejic.201601440

upstream raw materials:

(ScRp)-PPFOAc