[Ni(SC₆H₄Me-4)(triphos)]BPh₄

Base Information

Chemical Name:[Ni(SC₆H₄Me-4)(triphos)]BPh₄
CAS No.:704903-67-3
Molecular Formula:C₂₄H₂₀B*C₄₁H₄₀NiP₃S
Molecular Weight:1035.68
Hs Code.:

[Ni(SC<sub>6</sub>H<sub>4</sub>Me-4)(triphos)]BPh<sub>4</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ni(SC₆H₄Me-4)(triphos)]BPh₄

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Technology Process of [Ni(SC₆H₄Me-4)(triphos)]BPh₄

There total 1 articles about [Ni(SC₆H₄Me-4)(triphos)]BPh₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 40326-49-6
[NiCl(bis(2-diphenylphosphinoethyl)phenylphosphine)](tetraphenylborate)

: 10486-08-5
sodium p-thiocresolate

: 704903-67-3
[Ni(SC₆H₄Me-4)(triphos)]BPh₄

Guidance literature:: In tetrahydrofuran; Na-salt was added to stirred soln. of Ni-complex in THF, stirred at roomtemp. for 1 h under N2; concd., MeOH was added, filtered, washed with MeOH, dried in vacuo, recrystd. from CH2Cl2/MeOH; elem. anal.;
DOI:10.1021/ic0303237

Reference yield:

: 164164-16-3
2,6-lutidinium tetraphenylborate

: 704903-67-3
[Ni(SC₆H₄Me-4)(triphos)]BPh₄

: [Ni(SC₆H₄Me-4)(triphos)]H⁽²⁺⁾

Guidance literature:: In acetonitrile; Ni-complex was reacted with (2,6-dimethylpyridine)BPh4 in MeCN at 25°C under N2; monitored by NMR; Kinetics;
DOI:10.1021/ic0303237