N,N-diisopropyl P,P-diphenylphosphinamine P-1borane

Base Information

Chemical Name:N,N-diisopropyl P,P-diphenylphosphinamine P-1borane
CAS No.:1394286-58-8
Molecular Formula:C₁₈H₂₇BNP
Molecular Weight:299.204
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diisopropyl P,P-diphenylphosphinamine P-1borane

Chemical Property:

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Technology Process of N,N-diisopropyl P,P-diphenylphosphinamine P-1borane

There total 6 articles about N,N-diisopropyl P,P-diphenylphosphinamine P-1borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1394286-58-8
N,N-diisopropyl P,P-diphenylphosphinamine P-1borane

Guidance literature:

Reference yield:

: 1394286-57-7
chloro(diisopropylamino)diphenyl-phosphonium chloride

: 1394286-58-8
N,N-diisopropyl P,P-diphenylphosphinamine P-1borane

Guidance literature:: With sodium tetrahydroborate; In diethylene glycol dimethyl ether; toluene; at 70 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201302907

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1394286-58-8
N,N-diisopropyl P,P-diphenylphosphinamine P-1borane

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / diethyl ether / 3 h / 0 °C / Schlenk technique; Inert atmosphere

2: dihydrogen peroxide / water / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

3: oxalyl dichloride / toluene / 20 - 70 °C / Inert atmosphere; Schlenk technique

4: sodium tetrahydroborate / toluene; diethylene glycol dimethyl ether / 1 h / 70 °C / Inert atmosphere; Schlenk technique

With sodium tetrahydroborate; oxalyl dichloride; dihydrogen peroxide; triethylamine; In diethyl ether; diethylene glycol dimethyl ether; water; toluene;
DOI:10.1002/chem.201302907