MoI₂(CO)3(P(C₆H₅)(C₆H₁₁)2)(As(C₆H₅)3)

Base Information

• Chemical Name: MoI₂(CO)3(P(C₆H₅)(C₆H₁₁)2)(As(C₆H₅)3)
• CAS No.: 118519-08-7
• Molecular Formula: C₃₉H₄₂AsI₂MoO₃P
• Molecular Weight: 1014.41
• Mol file: 118519-08-7.mol

Synonyms:

Chemical Property of MoI₂(CO)3(P(C₆H₅)(C₆H₁₁)2)(As(C₆H₅)3)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of MoI₂(CO)3(P(C₆H₅)(C₆H₁₁)2)(As(C₆H₅)3)

There total 1 articles about MoI₂(CO)3(P(C₆H₅)(C₆H₁₁)2)(As(C₆H₅)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

MoI2(CO)3(MeCN)2 (102349-56-4) + triphenyl-arsane (603-32-7) + dicyclohexylphenylphosphine (6476-37-5) → MoI2(CO)3(P(C6H5)(C6H11)2)(As(C6H5)3) (118519-08-7)

Guidance literature:

In dichloromethane; byproducts: NCMe; under N2; AsPh3 added to Mo-complex in CH2Cl2 at 25°C; stirred for 3 min; PPh(C6H11)2 added; stirred for 27 min;; filtration; removal of solvent (vacuum); recrystn. from CH2Cl2; elem. anal.;;

DOI:10.1039/DT9880002729

upstream raw materials:

MoI₂(CO)3(MeCN)2

triphenyl-arsane

dicyclohexylphenylphosphine