({[(dioctadecylcarbamoylmethylcarbamoyl)methyl]carbamoyl}methyl)carbamic acid 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(1-benzyloxymethyl-2-benzyloxyethoxymethyl)propyl ester

Base Information

Chemical Name:({[(dioctadecylcarbamoylmethylcarbamoyl)methyl]carbamoyl}methyl)carbamic acid 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(1-benzyloxymethyl-2-benzyloxyethoxymethyl)propyl ester
CAS No.:939427-95-9
Molecular Formula:C₈₁H₁₂₈N₄O₁₁
Molecular Weight:1333.93
Hs Code.:

({[(dioctadecylcarbamoylmethylcarbamoyl)methyl]carbamoyl}methyl)carbamic acid 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(1-benzyloxymethyl-2-benzyloxyethoxymethyl)propyl ester

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Chemical Property of ({[(dioctadecylcarbamoylmethylcarbamoyl)methyl]carbamoyl}methyl)carbamic acid 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(1-benzyloxymethyl-2-benzyloxyethoxymethyl)propyl ester

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Technology Process of ({[(dioctadecylcarbamoylmethylcarbamoyl)methyl]carbamoyl}methyl)carbamic acid 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(1-benzyloxymethyl-2-benzyloxyethoxymethyl)propyl ester

There total 7 articles about ({[(dioctadecylcarbamoylmethylcarbamoyl)methyl]carbamoyl}methyl)carbamic acid 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(1-benzyloxymethyl-2-benzyloxyethoxymethyl)propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₄₅ClO₈

: 2-amino-N-[(dioctadecylcarbamoylmethylcarbamoyl)methyl]acetamide trifluoroacetic acid salt

: 939427-95-9
({[(dioctadecylcarbamoylmethylcarbamoyl)methyl]carbamoyl}methyl)carbamic acid 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(1-benzyloxymethyl-2-benzyloxyethoxymethyl)propyl ester

Guidance literature:: With diisopropylamine; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/j.bmc.2007.02.037

Reference yield:

: 939427-91-5
({[(dioctadecylcarbamoylmethylcarbamoyl)methyl]carbamoyl}methyl)carbamic acid tert-butyl ester

: 939427-95-9
({[(dioctadecylcarbamoylmethylcarbamoyl)methyl]carbamoyl}methyl)carbamic acid 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(1-benzyloxymethyl-2-benzyloxyethoxymethyl)propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 2 h / 20 °C

2: 350 mg / diisopropylamine / tetrahydrofuran / 24 h / 20 °C

With diisopropylamine; In tetrahydrofuran;
DOI:10.1016/j.bmc.2007.02.037

Reference yield:

: 112-99-2
Dioctadecylamine

: 939427-95-9
({[(dioctadecylcarbamoylmethylcarbamoyl)methyl]carbamoyl}methyl)carbamic acid 3-(2-benzyloxy-1-(benzyloxymethyl)ethoxy)-2-(1-benzyloxymethyl-2-benzyloxyethoxymethyl)propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / triethylamine; (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium PF₆ / CHCl₃ / 4 h / 20 °C

2: 92 percent / 2 h / 20 °C

3: 350 mg / diisopropylamine / tetrahydrofuran / 24 h / 20 °C

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; diisopropylamine; In tetrahydrofuran; chloroform;
DOI:10.1016/j.bmc.2007.02.037