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Technology Process of <1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester

<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester

Base Information
  • Chemical Name:<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester
  • CAS No.:120665-69-2
  • Molecular Formula:C23H36O3S
  • Molecular Weight:392.603
  • Hs Code.:
<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester

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Chemical Property of <1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester
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Technology Process of <1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester

There total 2 articles about <1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-6-hydroxy-1,4a-dimethyl-7-(1-methylethyl)-1-phenanthrencarbonsaeure-methylester
3484-53-5

<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-6-hydroxy-1,4a-dimethyl-7-(1-methylethyl)-1-phenanthrencarbonsaeure-methylester

acetic anhydride
108-24-7

acetic anhydride

<1R-(1α,4aβ,4bα,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-oxo-1-phenanthrencarbonsaeure-methylester
55623-34-2

<1R-(1α,4aβ,4bα,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-oxo-1-phenanthrencarbonsaeure-methylester

<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester
120665-69-2

<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester

<1R-(1α,4aβ,4bα,6α,10aα)>-6-Acetoxy-1,2,3,4,4a,4b,5,6,10,10a-decahydro-1,4a-dimethyl-7-(1-methylethyl)-1-phenanthrencarbonsaeure-methylester
6821-61-0

<1R-(1α,4aβ,4bα,6α,10aα)>-6-Acetoxy-1,2,3,4,4a,4b,5,6,10,10a-decahydro-1,4a-dimethyl-7-(1-methylethyl)-1-phenanthrencarbonsaeure-methylester

Guidance literature:
In dimethyl sulfoxide; for 30h; Ambient temperature;

Reference yield: 12.0%

<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-6-hydroxy-1,4a-dimethyl-7-(1-methylethyl)-1-phenanthrencarbonsaeure-methylester
3484-53-5

<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-6-hydroxy-1,4a-dimethyl-7-(1-methylethyl)-1-phenanthrencarbonsaeure-methylester

dimethyl sulfoxide
67-68-5,8070-53-9

dimethyl sulfoxide

<1R-(1α,4aβ,4bα,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-oxo-1-phenanthrencarbonsaeure-methylester
55623-34-2

<1R-(1α,4aβ,4bα,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-oxo-1-phenanthrencarbonsaeure-methylester

<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester
120665-69-2

<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-1,4a-dimethyl-7-(1-methylethyl)-6-(methylthiomethoxy)-1-phenanthrencarbonsaeure-methylester

<1R-(1α,4aβ,4bα,6α,10aα)>-6-Acetoxy-1,2,3,4,4a,4b,5,6,10,10a-decahydro-1,4a-dimethyl-7-(1-methylethyl)-1-phenanthrencarbonsaeure-methylester
6821-61-0

<1R-(1α,4aβ,4bα,6α,10aα)>-6-Acetoxy-1,2,3,4,4a,4b,5,6,10,10a-decahydro-1,4a-dimethyl-7-(1-methylethyl)-1-phenanthrencarbonsaeure-methylester

Guidance literature:
With acetic anhydride; for 30h; Ambient temperature;
upstream raw materials:

<1R-(1α,4aβ,4bα,6α,10aα)>-1,2,3,4,4a,4b,5,6,10,10a-Decahydro-6-hydroxy-1,4a-dimethyl-7-(1-methylethyl)-1-phenanthrencarbonsaeure-methylester

acetic anhydride

dimethyl sulfoxide

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