N⁴-benzoyl-5'-O-(4,4'-dimethoxytrityl)-3'-O-[(N,N-diisopropylamino)(2-cyanoethyloxy)phosphinyl]-2'-O-[4-(N-dichloroacetyl-N-methylamino)benzyloxy]methylcytidine

Base Information

• Chemical Name: N⁴-benzoyl-5'-O-(4,4'-dimethoxytrityl)-3'-O-[(N,N-diisopropylamino)(2-cyanoethyloxy)phosphinyl]-2'-O-[4-(N-dichloroacetyl-N-methylamino)benzyloxy]methylcytidine
• CAS No.: 1020100-96-2
• Molecular Formula: C₅₇H₆₃Cl₂N₆O₁₁P
• Molecular Weight: 1110.04

Synonyms:

Chemical Property of N⁴-benzoyl-5'-O-(4,4'-dimethoxytrityl)-3'-O-[(N,N-diisopropylamino)(2-cyanoethyloxy)phosphinyl]-2'-O-[4-(N-dichloroacetyl-N-methylamino)benzyloxy]methylcytidine

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of N⁴-benzoyl-5'-O-(4,4'-dimethoxytrityl)-3'-O-[(N,N-diisopropylamino)(2-cyanoethyloxy)phosphinyl]-2'-O-[4-(N-dichloroacetyl-N-methylamino)benzyloxy]methylcytidine

There total 1 articles about N⁴-benzoyl-5'-O-(4,4'-dimethoxytrityl)-3'-O-[(N,N-diisopropylamino)(2-cyanoethyloxy)phosphinyl]-2'-O-[4-(N-dichloroacetyl-N-methylamino)benzyloxy]methylcytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5'-O-(4,4'-dimethoxytrityl)-N4-benzoyl-2'-O-[4-(N-dichloroacetyl-N-methylamino)benzyloxy]methylcytidine (1020100-93-9) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → N4-benzoyl-5'-O-(4,4'-dimethoxytrityl)-3'-O-[(N,N-diisopropylamino)(2-cyanoethyloxy)phosphinyl]-2'-O-[4-(N-dichloroacetyl-N-methylamino)benzyloxy]methylcytidine (1020100-96-2)

Guidance literature:

With triethylamine; In dichloromethane; at 25 ℃; for 2h;

DOI:10.1021/jo702717g

upstream raw materials:

5'-O-(4,4'-dimethoxytrityl)-N⁴-benzoyl-2'-O-[4-(N-dichloroacetyl-N-methylamino)benzyloxy]methylcytidine

2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

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