(S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-2-(4-phenyl-[1,2,3]triazol-1-yl)-N1-prop-2-ynyl-succinamide

Base Information

Chemical Name:(S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-2-(4-phenyl-[1,2,3]triazol-1-yl)-N1-prop-2-ynyl-succinamide
CAS No.:1189342-40-2
Molecular Formula:C₃₂H₃₇N₉O₁₀
Molecular Weight:707.7
Hs Code.:

(S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-2-(4-phenyl-[1,2,3]triazol-1-yl)-N1-prop-2-ynyl-succinamide

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Chemical Property of (S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-2-(4-phenyl-[1,2,3]triazol-1-yl)-N1-prop-2-ynyl-succinamide

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Technology Process of (S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-2-(4-phenyl-[1,2,3]triazol-1-yl)-N1-prop-2-ynyl-succinamide

There total 1 articles about (S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-2-(4-phenyl-[1,2,3]triazol-1-yl)-N1-prop-2-ynyl-succinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1189342-38-8
(S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-2-(4-phenyl-[1,2,3]triazol-1-yl)-N1-(3-triisopropylsilyl-prop-2-ynyl)-succinamide

: 1189342-40-2
(S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-2-(4-phenyl-[1,2,3]triazol-1-yl)-N1-prop-2-ynyl-succinamide

Guidance literature:: (S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-2-(4-phenyl-[1,2,3]triazol-1-yl)-N1-(3-triisopropylsilyl-prop-2-ynyl)-succinamide; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

With hydrogenchloride; water; In tetrahydrofuran;
DOI:10.1016/j.tet.2009.06.093

Reference yield:

: 6926-44-9
phenethyl azide

: 1189342-40-2
(S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-2-(4-phenyl-[1,2,3]triazol-1-yl)-N1-prop-2-ynyl-succinamide

: 1189342-41-3
(S)-N4-([1-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl]-[1,2,3]triazol-4-yl]methyl)-N1-[(1-phenethyl-1H-[1,2,3]triazol-4-yl)methyl]-2-(4-phenyl-[1,2,3]triazol-1-yl)-succinamide

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.06.093