dicarbonylbis(trimethylphosphite)diphenylketene iron

Base Information

Chemical Name:dicarbonylbis(trimethylphosphite)diphenylketene iron
CAS No.:125963-16-8
Molecular Formula:C₂₂H₂₈FeO₉P₂
Molecular Weight:554.253
Hs Code.:

Synonyms:

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Chemical Property of dicarbonylbis(trimethylphosphite)diphenylketene iron

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Technology Process of dicarbonylbis(trimethylphosphite)diphenylketene iron

There total 3 articles about dicarbonylbis(trimethylphosphite)diphenylketene iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79110-70-6
mu.-dinitrogenbis(dicarbonylbis(trimethylphosphite)iron)

: 525-06-4
diphenyl ketene

: 125963-16-8,125994-63-0
dicarbonylbis(trimethylphosphite)diphenylketene iron

Guidance literature:: In diethyl ether; byproducts: N2; under Ar or N2, addn. of diphenylketene to a soln. of Fe-compd. in diethyl ether at -20°C, stirred at room temp. for 4 h; removal of solvent, extn. (pentane); elem. anal.;
DOI:10.1016/0022-328X(89)87232-8

Reference yield:

: 52155-11-0,1174574-37-8,26623-61-0
(CO)2Fe{P(OCH₃)3}2I₂

: 125963-16-8,125994-63-0
dicarbonylbis(trimethylphosphite)diphenylketene iron

Guidance literature:: Multi-step reaction with 3 steps

1: sodium; CO / diethyl ether

2: nitrogen / diethyl ether

3: diethyl ether

With sodium; CO; nitrogen; In diethyl ether;
DOI:10.1016/0022-328X(89)87232-8

Reference yield:

: 19457-84-2,14949-85-0
tricarbonylbis(trimethylphosphite)iron

: 125963-16-8,125994-63-0
dicarbonylbis(trimethylphosphite)diphenylketene iron

Guidance literature:: Multi-step reaction with 2 steps

1: nitrogen / diethyl ether

2: diethyl ether

With nitrogen; In diethyl ether;
DOI:10.1016/0022-328X(89)87232-8