(4,7-dihydro-5,6-dimethylisobenzofuran-1,3-diyl)bis(benzene-p-decanoic acid)

Base Information

• Chemical Name: (4,7-dihydro-5,6-dimethylisobenzofuran-1,3-diyl)bis(benzene-p-decanoic acid)
• CAS No.: 84543-16-8
• Molecular Formula: C₄₂H₅₆O₅
• Molecular Weight: 640.904
• Mol file: 84543-16-8.mol

Synonyms:

Chemical Property of (4,7-dihydro-5,6-dimethylisobenzofuran-1,3-diyl)bis(benzene-p-decanoic acid)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4,7-dihydro-5,6-dimethylisobenzofuran-1,3-diyl)bis(benzene-p-decanoic acid)

There total 6 articles about (4,7-dihydro-5,6-dimethylisobenzofuran-1,3-diyl)bis(benzene-p-decanoic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-ethoxycarbonylnonanoic acid chloride (6946-46-9) → (4,7-dihydro-5,6-dimethylisobenzofuran-1,3-diyl)bis(benzene-p-decanoic acid) (84543-16-8)

Guidance literature:

Multi-step reaction with 6 steps

1: AlCl₃

2: H₂, 2percent HCl / 5percent Pd-C / acetic acid

3: AlCl₃ / CH₂Cl₂

4: benzene / Heating

5: p-TosOH / benzene / Heating

6: 0.5 M KOH / ethanol / Heating

With hydrogenchloride; potassium hydroxide; aluminium trichloride; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid; benzene;

DOI:10.1039/c39820001147

Reference yield:

10-oxo-10-phenyl-decanoic acid ethyl ester (84543-12-4) → (4,7-dihydro-5,6-dimethylisobenzofuran-1,3-diyl)bis(benzene-p-decanoic acid) (84543-16-8)

Guidance literature:

Multi-step reaction with 5 steps

1: H₂, 2percent HCl / 5percent Pd-C / acetic acid

2: AlCl₃ / CH₂Cl₂

3: benzene / Heating

4: p-TosOH / benzene / Heating

5: 0.5 M KOH / ethanol / Heating

With hydrogenchloride; potassium hydroxide; aluminium trichloride; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid; benzene;

DOI:10.1039/c39820001147

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → (4,7-dihydro-5,6-dimethylisobenzofuran-1,3-diyl)bis(benzene-p-decanoic acid) (84543-16-8)

Guidance literature:

Multi-step reaction with 6 steps

1: AlCl₃

2: H₂, 2percent HCl / 5percent Pd-C / acetic acid

3: AlCl₃ / CH₂Cl₂

4: benzene / Heating

5: p-TosOH / benzene / Heating

6: 0.5 M KOH / ethanol / Heating

With hydrogenchloride; potassium hydroxide; aluminium trichloride; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid; benzene;

DOI:10.1039/c39820001147

upstream raw materials:

9-ethoxycarbonylnonanoic acid chloride

10-phenyl-decanoic acid ethyl ester

10-oxo-10-phenyl-decanoic acid ethyl ester

10-(4-{(E)-4-[4-(9-Ethoxycarbonyl-nonyl)-phenyl]-4-oxo-but-2-enoyl}-phenyl)-decanoic acid ethyl ester

Refernces