AlMe₂[3,5-Bu(t)2-2-(O)C₆H₂CH=N-2-PPh₂C₆H₄]

Base Information

Chemical Name:AlMe₂[3,5-Bu(t)2-2-(O)C₆H₂CH=N-2-PPh₂C₆H₄]
CAS No.:426841-62-5
Molecular Formula:C₃₅H₄₁AlNOP
Molecular Weight:549.672
Hs Code.:

AlMe<sub>2</sub>[3,5-Bu(t)2-2-(O)C<sub>6</sub>H<sub>2</sub>CH=N-2-PPh<sub>2</sub>C<sub>6</sub>H<sub>4</sub>]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of AlMe₂[3,5-Bu(t)2-2-(O)C₆H₂CH=N-2-PPh₂C₆H₄]

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Technology Process of AlMe₂[3,5-Bu(t)2-2-(O)C₆H₂CH=N-2-PPh₂C₆H₄]

There total 1 articles about AlMe₂[3,5-Bu(t)2-2-(O)C₆H₂CH=N-2-PPh₂C₆H₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 75-24-1
trimethylaluminum

: 426841-61-4
2-((2′-(diphenylphosphino)phenylimino)methyl)-4,6-di-tert-butylphenol

: 426841-62-5
AlMe₂[3,5-Bu(t)2-2-(O)C₆H₂CH=N-2-PPh₂C₆H₄]

Guidance literature:: In toluene; byproducts: CH4; (N2); standard Schlenk technique; Me3Al in toluene was added dropwise tosoln. of ligand in toluene; mixt. was refluxed for 12 h; volatiles removed (vac.); extd. (MeCN); cooled and kept for 1-2 d at ambient temp.; elem. anal.;
DOI:10.1039/b106131n

Reference yield:

: 426841-62-5
AlMe₂[3,5-Bu(t)2-2-(O)C₆H₂CH=N-2-PPh₂C₆H₄]

: 1109-15-5
tris(pentafluorophenyl)borate

: 426841-65-8
(AlMe[3,5-Bu(t)2-2-(O)C₆H₂CH=N-2-PPh₂C₆H₄])(MeB(C₆F₅)3)

Guidance literature:: In benzene-d6; (N2); standard Schlenk technique; soln. of B(C6F5)3 (1 equiv.) in C6D6 was added dropwise to shaken soln. of Al complex in C6D6; kept for 0.5 h; C6D6 soln. decanted; residue dissolved in CD2Cl2; NMR monitoring;
DOI:10.1039/b106131n