Benzyl-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosyl)-(1->3)-O-(4-O-acetyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

Base Information

Chemical Name:Benzyl-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosyl)-(1->3)-O-(4-O-acetyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid
CAS No.:113879-95-1
Molecular Formula:C₃₇H₄₈O₁₃
Molecular Weight:700.78
Hs Code.:

Benzyl-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosyl)-(1->3)-O-(4-O-acetyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

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Chemical Property of Benzyl-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosyl)-(1->3)-O-(4-O-acetyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

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Technology Process of Benzyl-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosyl)-(1->3)-O-(4-O-acetyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

There total 4 articles about Benzyl-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosyl)-(1->3)-O-(4-O-acetyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 108-24-7
acetic anhydride

: 113879-94-0
Benzyl-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosyl)-(1->3)-O-(2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

: 113879-95-1
Benzyl-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosyl)-(1->3)-O-(4-O-acetyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

Guidance literature:: With pyridine; at 5 ℃; for 24h;
DOI:10.1016/0008-6215(87)80139-8

Reference yield:

: 78086-65-4
4-O-Acetyl-1,5-anhydro-2,6-didesoxy-3-C-methyl-D-ribo-hex-1-enit

: 113879-95-1
Benzyl-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosyl)-(1->3)-O-(4-O-acetyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 11 percent / N-iodosuccinimide, molecular sieves 3A, / acetonitrile; diethyl ether / 72 h

2: 67 percent / H₂, triethylamine / 10percent Pd-C / ethyl acetate / 4 h

3: 62 percent / pyridine / 24 h / 5 °C

With pyridine; N-iodo-succinimide; 3 A molecular sieve; hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethyl acetate; acetonitrile;
DOI:10.1016/0008-6215(87)80139-8

Reference yield:

: 94820-99-2
benzyl-4-O-benzoyl-3-O-(2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside

: 113879-95-1
Benzyl-O-(4-O-acetyl-2,6-didesoxy-3-C-methyl-α-D-ribo-hexopyranosyl)-(1->3)-O-(4-O-acetyl-2,6-didesoxy-β-D-arabino-hexopyranosyl)-(1->3)-4-O-benzoyl-2,6-didesoxy-β-D-arabino-hexopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 11 percent / N-iodosuccinimide, molecular sieves 3A, / acetonitrile; diethyl ether / 72 h

2: 67 percent / H₂, triethylamine / 10percent Pd-C / ethyl acetate / 4 h

3: 62 percent / pyridine / 24 h / 5 °C

With pyridine; N-iodo-succinimide; 3 A molecular sieve; hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethyl acetate; acetonitrile;
DOI:10.1016/0008-6215(87)80139-8