(2S)-N-{4-[5-[2-methoxy-4-[(E)-3-morpholino-3-oxo-1-propenyl]phenoxy]pentyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

Base Information

• Chemical Name: (2S)-N-{4-[5-[2-methoxy-4-[(E)-3-morpholino-3-oxo-1-propenyl]phenoxy]pentyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal
• CAS No.: 1246890-28-7
• Molecular Formula: C₃₆H₄₉N₃O₉S₂
• Molecular Weight: 731.932

Synonyms:

Chemical Property of (2S)-N-{4-[5-[2-methoxy-4-[(E)-3-morpholino-3-oxo-1-propenyl]phenoxy]pentyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of (2S)-N-{4-[5-[2-methoxy-4-[(E)-3-morpholino-3-oxo-1-propenyl]phenoxy]pentyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

There total 1 articles about (2S)-N-{4-[5-[2-methoxy-4-[(E)-3-morpholino-3-oxo-1-propenyl]phenoxy]pentyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

5-(4'-hydroxy-3'-methoxy-phenyl)-2E-propenoic acid morpholine amide (55882-77-4) + (2S)-N-[4-(5-bromopentyloxy)-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethyl thioacetal (343308-57-6) → (2S)-N-{4-[5-[2-methoxy-4-[(E)-3-morpholino-3-oxo-1-propenyl]phenoxy]pentyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal (1246890-28-7)

Guidance literature:

With potassium carbonate; In acetonitrile; for 12h; Reflux;

DOI:10.1016/j.ejmech.2010.05.041

Reference yield:

(2S)-N-{4-[5-[2-methoxy-4-[(E)-3-morpholino-3-oxo-1-propenyl]phenoxy]pentyloxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal (1246890-28-7) → C36H51N3O7S2

Guidance literature:

With tin(II) chloride hydrate; In methanol; Reflux;

DOI:10.1016/j.ejmech.2010.05.041

upstream raw materials:

5-(4'-hydroxy-3'-methoxy-phenyl)-2E-propenoic acid morpholine amide

(2S)-N-[4-(5-bromopentyloxy)-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethyl thioacetal

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