2-Propenoyl azide, 3-(2-nitrophenyl)-

Base Information

• Chemical Name: 2-Propenoyl azide, 3-(2-nitrophenyl)-
• CAS No.: 105884-24-0
• Molecular Formula: C9H6N4O3
• Molecular Weight: 218.172
• Mol file: 105884-24-0.mol

Synonyms:

Chemical Property of 2-Propenoyl azide, 3-(2-nitrophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Propenoyl azide, 3-(2-nitrophenyl)-

There total 1 articles about 2-Propenoyl azide, 3-(2-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitro-cinnamoyl chloride (141236-47-7,52162-78-4) → C9H6N4O3 (105884-24-0)

Guidance literature:

With sodium azide; In acetone; at 20 ℃; Cooling with ice;

DOI:10.1021/jo101394c

Reference yield: 58.0%

C9H6N4O3 (105884-24-0) → 3,5-bis(2-nitrophenyl)pyridine (1246767-46-3)

Guidance literature:

With acetic acid; In dimethyl sulfoxide; at 150 ℃; for 4h; Inert atmosphere;

DOI:10.1021/jo101394c

upstream raw materials:

2-nitro-cinnamoyl chloride

Downstream raw materials:

3,5-bis(2-nitrophenyl)pyridine

Refernces