Benzyl-3,4-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-desoxy-6-O--α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-3,4-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-desoxy-6-O--α-D-glucopyranosid
CAS No.:104845-94-5
Molecular Formula:C₅₂H₅₉NO₁₈
Molecular Weight:986.036
Hs Code.:

Benzyl-3,4-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-desoxy-6-O-<methyl-(4,5,7,8-tetra-O-acetyl-3-desoxy-α,β-D-manno-2-octulopyranosyl)onat>-α-D-glucopyranosid

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Chemical Property of Benzyl-3,4-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-desoxy-6-O--α-D-glucopyranosid

Chemical Property:

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Technology Process of Benzyl-3,4-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-desoxy-6-O--α-D-glucopyranosid

There total 8 articles about Benzyl-3,4-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-desoxy-6-O--α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 57690-71-8
Benzyl-3,4-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-desoxy-α-D-glucopyranosid

: 148152-74-3
methyl (4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosyl bromide)onate

: 104845-94-5
(2R,4R,5R,6R)-4,5-Diacetoxy-6-((S)-1,2-diacetoxy-ethyl)-2-((2R,3S,4R,5R,6S)-3,4,6-tris-benzyloxy-5-benzyloxycarbonylamino-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-2-carboxylic acid methyl ester

Guidance literature:: With mercury dibromide; In dichloromethane; toluene;
DOI:10.1016/S0040-4039(00)84197-0

Reference yield:

: 57690-71-8
Benzyl-3,4-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-desoxy-α-D-glucopyranosid

: 104845-94-5
Benzyl-3,4-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-desoxy-6-O--α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) HgBr₂, molecular sieve 4 Angstroem; 2.) NaOMe (1M) / 1.) toluene, CH₂Cl₂, 88 h, room temp.; 2.) CH₃OH, 2.5 h

2: DMAP / pyridine / 2 h

With dmap; 4 A molecular sieve; sodium methylate; mercury dibromide; In pyridine;

Reference yield:

: 85382-87-2
methyl (4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-oct-2-ulopyranosyl bromide)onate

: 104845-94-5
Benzyl-3,4-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-desoxy-6-O--α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) HgBr₂, molecular sieve 4 Angstroem; 2.) NaOMe (1M) / 1.) toluene, CH₂Cl₂, 88 h, room temp.; 2.) CH₃OH, 2.5 h

2: DMAP / pyridine / 2 h

With dmap; 4 A molecular sieve; sodium methylate; mercury dibromide; In pyridine;