C₃₂H₃₀Cl₂O₆

Base Information

• Chemical Name: C₃₂H₃₀Cl₂O₆
• CAS No.: 1309661-29-7
• Molecular Formula: C₃₂H₃₀Cl₂O₆
• Molecular Weight: 581.493
• Mol file: 1309661-29-7.mol

Synonyms:

Chemical Property of C₃₂H₃₀Cl₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₃₀Cl₂O₆

There total 5 articles about C₃₂H₃₀Cl₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(benzyloxy)-4-(bromomethyl)-2-methoxybenzene (72724-00-6) + sodium trichloroacetate (650-51-1) → C32H30Cl2O6 (1309661-29-7)

Guidance literature:

With tetrabutylammomium bromide; In tetrahydrofuran; at 60 ℃; for 24h;

DOI:10.1002/anie.201100495

Reference yield:

3-methoxy-4-(phenylmethoxy)benzaldehyde (2426-87-1) → C32H30Cl2O6 (1309661-29-7)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium tetrahydroborate / tetrahydrofuran; methanol / 2 h / 20 °C

2: phosphorus tribromide / dichloromethane / 0 - 20 °C

3: tetrabutylammomium bromide / tetrahydrofuran / 24 h / 60 °C

With sodium tetrahydroborate; tetrabutylammomium bromide; phosphorus tribromide; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1002/anie.201100495

Reference yield:

4-benzyloxy-3-methoxybenzyl alcohol (33693-48-0) → C32H30Cl2O6 (1309661-29-7)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus tribromide / dichloromethane / 0 - 20 °C

2: tetrabutylammomium bromide / tetrahydrofuran / 24 h / 60 °C

With tetrabutylammomium bromide; phosphorus tribromide; In tetrahydrofuran; dichloromethane;

DOI:10.1002/anie.201100495

upstream raw materials:

3-methoxy-4-(phenylmethoxy)benzaldehyde

1-(benzyloxy)-4-(bromomethyl)-2-methoxybenzene

sodium trichloroacetate

4-benzyloxy-3-methoxybenzyl alcohol

Downstream raw materials:

C₁₇H₁₆Cl₂O₄

C₂₇H₂₆Cl₂N₂O₄