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((C6H11)6Si6O11NbOC2H5)2

Base Information
  • Chemical Name:((C6H11)6Si6O11NbOC2H5)2
  • CAS No.:917988-41-1
  • Molecular Formula:C76H142Nb2O24Si12
  • Molecular Weight:1962.79
  • Hs Code.:
((C<sub>6</sub>H<sub>11</sub>)6Si<sub>6</sub>O<sub>11</sub>NbOC<sub>2</sub>H<sub>5</sub>)2

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Chemical Property of ((C6H11)6Si6O11NbOC2H5)2
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Technology Process of ((C6H11)6Si6O11NbOC2H5)2

There total 1 articles about ((C6H11)6Si6O11NbOC2H5)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In toluene; byproducts: C2H5OH; (dry N2 or Ar, Schlenk) Nb-compound was added to a soln. of siloxane-compound in toluene, the mixt. was stirred for 15 min followed by refluxingfor 1 h; 1/3 of the solvent was distilled off, the soln. was cooled to 5°Cfor 1 week; elem. anal.;
DOI:10.1021/om0606587
Guidance literature:
In tetrahydrofuran-d8; byproducts: (c-C6H11)6Si6O7(OH)4; prolonged standing in THF-d8 in an NMR tube;
DOI:10.1021/om0606587
upstream raw materials:

niobium (V) ethoxide

Cy6Si6O7(OH)4

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