C₅₉H₅₈O₁₁

Base Information

Chemical Name:C₅₉H₅₈O₁₁
CAS No.:101923-78-8
Molecular Formula:C₅₉H₅₈O₁₁
Molecular Weight:943.103
Hs Code.:

C<sub>59</sub>H<sub>58</sub>O<sub>11</sub>

Synonyms:

Suppliers and Price of C₅₉H₅₈O₁₁

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₉H₅₈O₁₁

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₉H₅₈O₁₁

There total 15 articles about C₅₉H₅₈O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 504-15-4
orcinol

: 101923-78-8
C₅₉H₅₈O₁₁

Guidance literature:: Multi-step reaction with 15 steps

1: 77 percent / K₂CO₃ / acetone / 24 h

2: 72 percent / 1.) 2 N PhLi 2.) 1,2-dibromoethane / diethyl ether / 1.) 110 h in dark; 2.) r.t., 3 h

3: 97 percent / Br₃B / CH₂Cl₂ / 1.5 h / Heating

4: 91 percent / K₂CO₃ / dimethylformamide / 15 h / 40 °C

5: 89.7 percent / 1.) Mg, 1,2-dibromoethane / 1.) THF, reflux, 0.5 h; 2.) THF, -10 deg C, 30 min

6: 91.5 percent / hydrogen / 10percent Pd/C / ethyl acetate

7: 1.) POCl₃ 2.) H₂O / 1.) r.t., 1.5 h; 2.) 40 h

8: 88 percent / K₂CO₃ / dimethylformamide / 24 h / 40 °C

9: 96 percent / sulfamic acid, NaClO₂ / H₂O; dioxane / 0.17 h

10: 95 percent / K₂CO₃ / acetone / 2 h

11: 91 percent / hydrogen / 10percent Pd/C / ethyl acetate / 760 Torr

12: 1.) SnCl₄ 2.) H₂O / 1.) CHCl₂, -30 deg C, 1.5 h

13: 93 percent / K₂CO₃ / dimethylformamide / 14 h / 50 °C

14: 78 percent / sulfamic acid, 80percent NaClO₂ / H₂O; dioxane / 0.17 h

15: 10.3 g / trifluoroacetic anhydride / CH₂Cl₂ / 24 h / 19 °C

With sodium chlorite; aminosulfonic acid; water; hydrogen; boron tribromide; tin(IV) chloride; potassium carbonate; magnesium; phenyllithium; ethylene dibromide; trifluoroacetic anhydride; trichlorophosphate; palladium on activated charcoal; In 1,4-dioxane; diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1002/hlca.19850680719

Reference yield:

: 2675-82-3
bromo-4-dimethoxy-3,5-toluene

: 101923-78-8
C₅₉H₅₈O₁₁

Guidance literature:: Multi-step reaction with 13 steps

1: 97 percent / Br₃B / CH₂Cl₂ / 1.5 h / Heating

2: 91 percent / K₂CO₃ / dimethylformamide / 15 h / 40 °C

3: 89.7 percent / 1.) Mg, 1,2-dibromoethane / 1.) THF, reflux, 0.5 h; 2.) THF, -10 deg C, 30 min

4: 91.5 percent / hydrogen / 10percent Pd/C / ethyl acetate

5: 1.) POCl₃ 2.) H₂O / 1.) r.t., 1.5 h; 2.) 40 h

6: 88 percent / K₂CO₃ / dimethylformamide / 24 h / 40 °C

7: 96 percent / sulfamic acid, NaClO₂ / H₂O; dioxane / 0.17 h

8: 95 percent / K₂CO₃ / acetone / 2 h

9: 91 percent / hydrogen / 10percent Pd/C / ethyl acetate / 760 Torr

10: 1.) SnCl₄ 2.) H₂O / 1.) CHCl₂, -30 deg C, 1.5 h

11: 93 percent / K₂CO₃ / dimethylformamide / 14 h / 50 °C

12: 78 percent / sulfamic acid, 80percent NaClO₂ / H₂O; dioxane / 0.17 h

13: 10.3 g / trifluoroacetic anhydride / CH₂Cl₂ / 24 h / 19 °C

With sodium chlorite; aminosulfonic acid; water; hydrogen; boron tribromide; tin(IV) chloride; potassium carbonate; magnesium; ethylene dibromide; trifluoroacetic anhydride; trichlorophosphate; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1002/hlca.19850680719

Reference yield:

: 4179-19-5
1,3-dimethoxy-5-methylbenzene

: 101923-78-8
C₅₉H₅₈O₁₁

Guidance literature:: Multi-step reaction with 14 steps

1: 72 percent / 1.) 2 N PhLi 2.) 1,2-dibromoethane / diethyl ether / 1.) 110 h in dark; 2.) r.t., 3 h

2: 97 percent / Br₃B / CH₂Cl₂ / 1.5 h / Heating

3: 91 percent / K₂CO₃ / dimethylformamide / 15 h / 40 °C

4: 89.7 percent / 1.) Mg, 1,2-dibromoethane / 1.) THF, reflux, 0.5 h; 2.) THF, -10 deg C, 30 min

5: 91.5 percent / hydrogen / 10percent Pd/C / ethyl acetate

6: 1.) POCl₃ 2.) H₂O / 1.) r.t., 1.5 h; 2.) 40 h

7: 88 percent / K₂CO₃ / dimethylformamide / 24 h / 40 °C

8: 96 percent / sulfamic acid, NaClO₂ / H₂O; dioxane / 0.17 h

9: 95 percent / K₂CO₃ / acetone / 2 h

10: 91 percent / hydrogen / 10percent Pd/C / ethyl acetate / 760 Torr

11: 1.) SnCl₄ 2.) H₂O / 1.) CHCl₂, -30 deg C, 1.5 h

12: 93 percent / K₂CO₃ / dimethylformamide / 14 h / 50 °C

13: 78 percent / sulfamic acid, 80percent NaClO₂ / H₂O; dioxane / 0.17 h

14: 10.3 g / trifluoroacetic anhydride / CH₂Cl₂ / 24 h / 19 °C

With sodium chlorite; aminosulfonic acid; water; hydrogen; boron tribromide; tin(IV) chloride; potassium carbonate; magnesium; phenyllithium; ethylene dibromide; trifluoroacetic anhydride; trichlorophosphate; palladium on activated charcoal; In 1,4-dioxane; diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1002/hlca.19850680719