[SP-4-1-(R(),R())]-(+/-)-rac-trans-bis[2-(methylphenylphosphino)ethanethiolato]palladium(II)

Base Information

Chemical Name:[SP-4-1-(R(*),R(*))]-(+/-)-rac-trans-bis[2-(methylphenylphosphino)ethanethiolato]palladium(II)
CAS No.:102850-02-2
Molecular Formula:C₁₈H₂₄P₂PdS₂
Molecular Weight:472.888
Hs Code.:

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Chemical Property of [SP-4-1-(R(*),R(*))]-(+/-)-rac-trans-bis[2-(methylphenylphosphino)ethanethiolato]palladium(II)

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Technology Process of [SP-4-1-(R(*),R(*))]-(+/-)-rac-trans-bis[2-(methylphenylphosphino)ethanethiolato]palladium(II)

There total 1 articles about [SP-4-1-(R(*),R(*))]-(+/-)-rac-trans-bis[2-(methylphenylphosphino)ethanethiolato]palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 21264-30-2,90243-59-7,14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 102782-08-1
(2-mercaptoethyl)methylphenylphosphine

: 102850-13-5
[SP-4-2-(R(*),S(*))]-(+/-)-meso-cis-bis[2-(methylphenylphosphino)ethanethiolato]palladium(II)

: 102782-04-7
[SP-4-1-(R(*),S(*))]-(+/-)-meso-trans-bis[2-(methylphenylphosphino)ethanethiolato]palladium(II)

: 102850-04-4
[SP-4-2-(R(*),R(*))]-(+/-)-rac-cis-bis[2-(methylphenylphosphino)ethanethiolato]palladium(II)

: 102850-02-2
[SP-4-1-(R(*),R(*))]-(+/-)-rac-trans-bis[2-(methylphenylphosphino)ethanethiolato]palladium(II)

Guidance literature:: With silver nitrate; triethylamine; In acetonitrile; byproducts: AgCl; react. of the Pd compd. with AgNO3 in MeCN in the dark under Ar (5 min), filtn. (AgCl), addn. of the phosphine and Et3N in MeCN and stirring for 30 min; stirring in MeOH at room temp. for 15 min, filtn., recrystn. of the undissolved from CH2Cl2-MeOH (after 4 h was the rac-cis compd. obtained), concn. of the MeOH extract and standing for 2 h (rac-trans compd.); elem.anal.;