Hmb-Gly-OBzl

Base Information

• Chemical Name: Hmb-Gly-OBzl
• CAS No.: 1033922-34-7
• Molecular Formula: C₁₇H₁₉NO₄
• Molecular Weight: 301.342
• Mol file: 1033922-34-7.mol

Synonyms:

Chemical Property of Hmb-Gly-OBzl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Hmb-Gly-OBzl

There total 1 articles about Hmb-Gly-OBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.9%

2-Hydroxy-4-methoxybenzaldehyde (673-22-3) + Gly-OBz (1738-68-7) → Hmb-Gly-OBzl (1033922-34-7)

Guidance literature:

2-Hydroxy-4-methoxybenzaldehyde; Gly-OBz; In ethanol;

With sodium tetrahydroborate; In ethanol; for 0.666667h; Further stages.; cooling;

DOI:10.1016/j.tetlet.2008.04.055

Reference yield:

Hmb-Gly-OBzl (1033922-34-7) + Fmoc-Val-OH (68858-20-8) → Fmoc-Val-HmbGly-OBzl (1033922-37-0)

Guidance literature:

With diisopropyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1016/j.tetlet.2008.04.055

upstream raw materials:

2-Hydroxy-4-methoxybenzaldehyde

Gly-OBz

Downstream raw materials:

Fmoc-Val-HmbGly-OBzl