carbonyl(chloro)bis(di-t-butylmethylphosphane)(E-2-phenylvinyl)ruthenium(II)

Base Information

Chemical Name:carbonyl(chloro)bis(di-t-butylmethylphosphane)(E-2-phenylvinyl)ruthenium(II)
CAS No.:122144-67-6
Molecular Formula:C₂₇H₄₉ClOP₂Ru
Molecular Weight:588.156
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Chemical Property of carbonyl(chloro)bis(di-t-butylmethylphosphane)(E-2-phenylvinyl)ruthenium(II)

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Technology Process of carbonyl(chloro)bis(di-t-butylmethylphosphane)(E-2-phenylvinyl)ruthenium(II)

There total 2 articles about carbonyl(chloro)bis(di-t-butylmethylphosphane)(E-2-phenylvinyl)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 69546-72-1,105015-57-4
carbonylchlorohydridobis(methyldi-t-butylphosphine)ruthenium(II)

: 536-74-3
phenylacetylene

: 122144-67-6
carbonyl(chloro)bis(di-t-butylmethylphosphane)(E-2-phenylvinyl)ruthenium(II)

Guidance literature:: In hexane; (N2); to suspn. of Ru complex was dropped PhCCH soln. and stirred at room temp. for 10 min; formed pptn. was filtered off, washed twice with hexane and dried in vac.; elem. anal.;

Reference yield:

: 105015-57-4
[HRuCl(CO)(P(C(CH₃)3)2CH₃)2]

: 536-74-3
phenylacetylene

: 122144-67-6
RuCl(CO){PCH₃(C(CH₃)3)2}2CHCHC₆H₅

Guidance literature:: In hexane; standard Schlenk and glovebox techniques, under prepurified Ar; addn. of phenylacetylene to the Ru-compd. in C6D6, react. within 15 min;

Reference yield: 81.0%

: 122144-67-6
carbonyl(chloro)bis(di-t-butylmethylphosphane)(E-2-phenylvinyl)ruthenium(II)

: 122144-68-7
dicarbonyl(chloro)bis(di-t-butylmethylphosphane)(E-2-phenylvinyl)ruthenium(II)

Guidance literature:: With CO; In benzene; (N2); into soln. of Ru complex was led CO for 2 min and stirred for 10 min at room temp.; filtered soln. was concd. in vac. and treated with MeOH, formed pptn. was filtered off, washed with MeOH and dried in vac.; elem. anal.;