p-tolylsulfonyl 3,4-epoxy 2-nonanol, erythro

Base Information

Chemical Name:p-tolylsulfonyl 3,4-epoxy 2-nonanol, erythro
CAS No.:116885-46-2
Molecular Formula:C₁₆H₂₄O₄S
Molecular Weight:312.43
Hs Code.:

Synonyms:

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Chemical Property of p-tolylsulfonyl 3,4-epoxy 2-nonanol, erythro

Chemical Property:

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Technology Process of p-tolylsulfonyl 3,4-epoxy 2-nonanol, erythro

There total 4 articles about p-tolylsulfonyl 3,4-epoxy 2-nonanol, erythro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107866-66-0
(E)-(S)-1-((R)-Toluene-4-sulfinyl)-non-3-en-2-ol

: 116949-51-0
p-tolylsulfonyl 3,4-epoxy 2-nonanol, threo

: 116885-46-2
p-tolylsulfonyl 3,4-epoxy 2-nonanol, erythro

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 8h; Yield given. Yields of byproduct given;

Reference yield:

: 2351-90-8,7367-82-0,42778-93-8
ethyl (2E)-oct-2-enoate

: 116885-46-2
p-tolylsulfonyl 3,4-epoxy 2-nonanol, erythro

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent

2: DIBAL / -78 °C

3: 1.) VO(Acac)2; 2.) 3 M t-butylhydroperoxide in toluene / CH₂Cl₂ / 12 h / 0 °C

With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; diisobutylaluminium hydride; In dichloromethane;

Reference yield:

: 1519-39-7
(R)-methyl p-tolyl sulfoxide

: 116885-46-2
p-tolylsulfonyl 3,4-epoxy 2-nonanol, erythro

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent

2: DIBAL / -78 °C

3: 1.) VO(Acac)2; 2.) 3 M t-butylhydroperoxide in toluene / CH₂Cl₂ / 12 h / 0 °C

With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; diisobutylaluminium hydride; In dichloromethane;