Technology Process of C24H26N2O7
There total 4 articles about C24H26N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
dimethyl 2-(1-(tert-butoxycarbonyl)pyrrolidine-2-carboxamido)biphenyl-4,4'-dicarboxylate;
With
potassium hydroxide;
In
tetrahydrofuran; water;
at 50 ℃;
for 19h;
With
hydrogenchloride;
In
water;
pH=4;
DOI:10.1021/ic502380q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 18 h / 2327.23 Torr
2.1: dmap; diisopropyl-carbodiimide / dichloromethane / 0.5 h / Cooling with ice
2.2: 40 h / 40 °C
3.1: water; potassium hydroxide / tetrahydrofuran / 16 h / 50 °C
With
dmap; palladium 10% on activated carbon; water; hydrogen; potassium hydroxide; diisopropyl-carbodiimide;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja202223d
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sulfuric acid; nitric acid / 5 °C / Cooling with ice
2.1: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 18 h / 2327.23 Torr
3.1: dmap; diisopropyl-carbodiimide / dichloromethane / 0.5 h / Cooling with ice
3.2: 40 h / 40 °C
4.1: water; potassium hydroxide / tetrahydrofuran / 16 h / 50 °C
With
dmap; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; nitric acid; potassium hydroxide; diisopropyl-carbodiimide;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja202223d
