C₂₆H₁₉NS

Base Information

Chemical Name:C₂₆H₁₉NS
CAS No.:1283741-53-6
Molecular Formula:C₂₆H₁₉NS
Molecular Weight:377.51
Hs Code.:

Synonyms:

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Chemical Property of C₂₆H₁₉NS

Chemical Property:

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Technology Process of C₂₆H₁₉NS

There total 4 articles about C₂₆H₁₉NS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 187731-56-2
4-(5H-dibenzo[b,f]azepin-5-yl)benzaldehyde

: 3462-99-5
[(thien-2-yl)methyl]triphenylphosphonium chloride

: 1283741-53-6
C₂₆H₁₉NS

Guidance literature:: 4-(5H-dibenzo[b,f]azepin-5-yl)benzaldehyde; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

[(thien-2-yl)methyl]triphenylphosphonium chloride; In tetrahydrofuran; at 20 ℃; for 25h; Inert atmosphere; Reflux;
DOI:10.1016/j.dyepig.2011.11.002

Reference yield:

: 78943-59-6
N-phenyldibenzazepine

: 1283741-53-6
C₂₆H₁₉NS

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 1 h / 0 °C / Inert atmosphere

1.2: 8 h / 80 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2.2: 25 h / 20 °C / Inert atmosphere; Reflux

With potassium tert-butylate; trichlorophosphate; In tetrahydrofuran; 1.1: Vilsmeier-Haack reaction / 1.2: Vilsmeier-Haack reaction / 2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1016/j.dyepig.2011.11.002

Reference yield:

: 591-50-4
iodobenzene

: 1283741-53-6
C₂₆H₁₉NS

Guidance literature:: Multi-step reaction with 3 steps

1.1: 18-crown-6 ether; copper; potassium carbonate / 1,2-dichloro-benzene / 48 h / 180 °C / Inert atmosphere

2.1: trichlorophosphate / 1 h / 0 °C / Inert atmosphere

2.2: 8 h / 80 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.2: 25 h / 20 °C / Inert atmosphere; Reflux

With 18-crown-6 ether; potassium tert-butylate; copper; potassium carbonate; trichlorophosphate; In tetrahydrofuran; 1,2-dichloro-benzene; 1.1: Ullmann condensation / 2.1: Vilsmeier-Haack reaction / 2.2: Vilsmeier-Haack reaction / 3.1: Wittig reaction / 3.2: Wittig reaction;
DOI:10.1016/j.dyepig.2011.11.002