C₂₃H₂₂N₆OS

Base Information

• Chemical Name: C₂₃H₂₂N₆OS
• CAS No.: 1355249-24-9
• Molecular Formula: C₂₃H₂₂N₆OS
• Molecular Weight: 430.533
• Mol file: 1355249-24-9.mol

Synonyms:

Chemical Property of C₂₃H₂₂N₆OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₂₂N₆OS

There total 2 articles about C₂₃H₂₂N₆OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C17H18N2O2 (1355249-20-5) → C23H22N6OS (1355249-24-9)

Guidance literature:

Multi-step reaction with 3 steps

1: phenyltrimethylammonium tribromide / chloroform / 2 h / Reflux

2: ethanol / 10 h / Reflux

3: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 4 h / Inert atmosphere; Reflux

With phenyltrimethylammonium tribromide; caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; ethanol; chloroform;

Reference yield:

C17H17BrN2O2 (1355249-21-6) → C23H22N6OS (1355249-24-9)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 10 h / Reflux

2: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 4 h / Inert atmosphere; Reflux

With caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; ethanol;

upstream raw materials:

C₁₇H₁₈N₂O₂

C₁₇H₁₇BrN₂O₂