Technology Process of C34(13)C4H61N7O10
There total 11 articles about C34(13)C4H61N7O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
2: N-ethyl-N,N-diisopropylamine / dichloromethane; acetonitrile / 72 h
3: trifluoroacetic acid / dichloromethane / 3 h
4: acetic anhydride / 3 h / 120 °C
5: acetonitrile / 60 h / Reflux
6: trifluoroacetic acid / dichloromethane / 3 h
With
acetic anhydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; acetonitrile;
DOI:10.1021/ja1097034
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane; acetonitrile / 72 h
2: trifluoroacetic acid / dichloromethane / 3 h
3: acetic anhydride / 3 h / 120 °C
4: acetonitrile / 60 h / Reflux
5: trifluoroacetic acid / dichloromethane / 3 h
With
acetic anhydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; acetonitrile;
DOI:10.1021/ja1097034
- Guidance literature:
-
Multi-step reaction with 7 steps
1: acetic anhydride
3: N-ethyl-N,N-diisopropylamine / dichloromethane; acetonitrile / 72 h
4: trifluoroacetic acid / dichloromethane / 3 h
5: acetic anhydride / 3 h / 120 °C
6: acetonitrile / 60 h / Reflux
7: trifluoroacetic acid / dichloromethane / 3 h
With
acetic anhydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; acetonitrile;
DOI:10.1021/ja1097034