1,11-bisamido>phenoxy>-3,6,9-trioxaundecane

Base Information

Chemical Name:1,11-bisamido>phenoxy>-3,6,9-trioxaundecane
CAS No.:74145-44-1
Molecular Formula:C₅₈H₆₆N₄O₁₉
Molecular Weight:1123.18
Hs Code.:

1,11-bis<o-<<o-(10-(o-nitrophenyl)-1,4,7,10-tetraoxadecyl)phenyl>amido>phenoxy>-3,6,9-trioxaundecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,11-bisamido>phenoxy>-3,6,9-trioxaundecane

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Technology Process of 1,11-bisamido>phenoxy>-3,6,9-trioxaundecane

There total 8 articles about 1,11-bisamido>phenoxy>-3,6,9-trioxaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 62107-77-1
tetraethylene glycol bis(2-aminophenyl)ether

: 344238-35-3
2-(2-{2-[2-(2-Nitro-phenoxy)-ethoxy]-ethoxy}-ethoxy)-benzoyl chloride

: 74145-44-1
1,11-bisamido>phenoxy>-3,6,9-trioxaundecane

Guidance literature:: In benzene; for 2h;

Reference yield:

: 88-75-5,78813-12-4
2-hydroxynitrobenzene

: 74145-44-1
1,11-bisamido>phenoxy>-3,6,9-trioxaundecane

Guidance literature:: Multi-step reaction with 6 steps

1: 72 percent / KOH / butan-1-ol; dimethylformamide / 20 h / Heating

2: pyridine / 0 - 5 °C

3: 1) NaOEt / 1) ethanol/DMF, 1) ethanol/DMF, 4 h, reflux

4: 97 percent / aq. KOH / ethanol / 0.33 h / Heating

5: SOCl₂

6: 65 percent / benzene / 2 h

With potassium hydroxide; thionyl chloride; sodium ethanolate; In pyridine; ethanol; N,N-dimethyl-formamide; butan-1-ol; benzene;

Reference yield:

: 31255-26-2
1-bromo-2-{2-[2-(2-bromoethoxy)ethoxy]-ethoxy}ethane

: 74145-44-1
1,11-bisamido>phenoxy>-3,6,9-trioxaundecane

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / KOH / butan-1-ol; dimethylformamide / 5 h / Heating

2: 74 percent / Raney nickel, 30percent aq. H₄N₂ solution / ethanol

3: 65 percent / benzene / 2 h

With potassium hydroxide; nickel; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide; butan-1-ol; benzene;