Technology Process of C15H18O4
There total 6 articles about C15H18O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,2-Bis(phenylsulfinyl)ethane; palladium diacetate; p-benzoquinone;
In
ethyl acetate;
at 20 ℃;
for 96h;
optical yield given as %de;
Molecular sieve;
DOI:10.1055/s-0031-1289549
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dichloromethane / 12 h / 20 °C
2: water; sodium hydroxide / methanol / 2 h / Reflux
3: 1,2-Bis(phenylsulfinyl)ethane; palladium diacetate; p-benzoquinone / ethyl acetate / 96 h / 20 °C / Molecular sieve
With
1,2-Bis(phenylsulfinyl)ethane; water; palladium diacetate; p-benzoquinone; sodium hydroxide;
In
methanol; dichloromethane; ethyl acetate;
DOI:10.1055/s-0031-1289549
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hexamethyldisilazane; N-(benzenesulfonyl)-3-phenyloxaziridine / tetrahydrofuran / 0.5 h / -78 °C
1.2: 1 h / 0 °C
2.1: dichloromethane / 12 h / 20 °C
3.1: water; sodium hydroxide / methanol / 2 h / Reflux
4.1: 1,2-Bis(phenylsulfinyl)ethane; palladium diacetate; p-benzoquinone / ethyl acetate / 96 h / 20 °C / Molecular sieve
With
1,2-Bis(phenylsulfinyl)ethane; water; palladium diacetate; sodium hexamethyldisilazane; N-(benzenesulfonyl)-3-phenyloxaziridine; p-benzoquinone; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1055/s-0031-1289549
