(2S,3S,4S)-N-hydroxy-2-phenyl-3,4-dicyanopyrrolidine

Base Information

Chemical Name:(2S,3S,4S)-N-hydroxy-2-phenyl-3,4-dicyanopyrrolidine
CAS No.:122950-59-8
Molecular Formula:C₁₂H₁₁N₃O
Molecular Weight:213.239
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4S)-N-hydroxy-2-phenyl-3,4-dicyanopyrrolidine

Chemical Property:

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Technology Process of (2S,3S,4S)-N-hydroxy-2-phenyl-3,4-dicyanopyrrolidine

There total 4 articles about (2S,3S,4S)-N-hydroxy-2-phenyl-3,4-dicyanopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₁₁H₁₈NOSi⁽¹⁺⁾*CF₃O₃S^(1-)

: 764-42-1
1,2-Dicyanoethylene

: 109800-96-6,109800-99-9,122950-59-8,122967-70-8
(3R,4R)-1-Hydroxy-2-phenyl-pyrrolidine-3,4-dicarbonitrile

Guidance literature:: With cesium fluoride; In 1,2-dimethoxyethane; Product distribution; other electron deficient alkenes;
DOI:10.1021/jo00226a050

Reference yield:

: 932-90-1
Benzaldoxime

: 109800-96-6,109800-99-9,122950-59-8,122967-70-8
(2S,3S,4S)-N-hydroxy-2-phenyl-3,4-dicyanopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 12 h / 0 °C

2: cesium fluoride / methanol

With cesium fluoride; In methanol;
DOI:10.1021/jo00279a036

Reference yield:

: 932-90-1
Benzaldoxime

: 109800-96-6,109800-99-9,122950-59-8,122967-70-8
(2R,3S,4S)-N-hydroxy-2-phenyl-3,4-dicyanopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 12 h / 0 °C

2: cesium fluoride / 1,2-dimethoxy-ethane

With cesium fluoride; In 1,2-dimethoxyethane;
DOI:10.1021/jo00279a036