{(R,R),(R)}/{(R,R),(S)}-(+/-)-(η5-cyclopentadienyl)(methylphenylphosphido){1,2-phenylenebis(methylphenylphosphine)}iron(II) monotetrahydrofuran solvate

Base Information

Chemical Name:{(R*,R*),(R*)}/{(R*,R*),(S*)}-(+/-)-(η5-cyclopentadienyl)(methylphenylphosphido){1,2-phenylenebis(methylphenylphosphine)}iron(II) monotetrahydrofuran solvate
CAS No.:122270-83-1
Molecular Formula:C₄H₈O*C₃₂H₃₃FeP₃
Molecular Weight:638.489
Hs Code.:

{(R*,R*),(R*)}/{(R*,R*),(S*)}-(+/-)-(η5-cyclopentadienyl)(methylphenylphosphido){1,2-phenylenebis(methylphenylphosphine)}iron(II) monotetrahydrofuran solvate

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Chemical Property of {(R*,R*),(R*)}/{(R*,R*),(S*)}-(+/-)-(η5-cyclopentadienyl)(methylphenylphosphido){1,2-phenylenebis(methylphenylphosphine)}iron(II) monotetrahydrofuran solvate

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Technology Process of {(R*,R*),(R*)}/{(R*,R*),(S*)}-(+/-)-(η5-cyclopentadienyl)(methylphenylphosphido){1,2-phenylenebis(methylphenylphosphine)}iron(II) monotetrahydrofuran solvate

There total 2 articles about {(R*,R*),(R*)}/{(R*,R*),(S*)}-(+/-)-(η5-cyclopentadienyl)(methylphenylphosphido){1,2-phenylenebis(methylphenylphosphine)}iron(II) monotetrahydrofuran solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 113572-54-6
{(R*,R*),(R*)}-(+/-)-(η5-cyclopentadienyl)(methylphenylphosphine){1,2-phenylenebis(methylphenylphosphine)}iron(II) hexafluorophosphate hemidichloromethane solvate

: 865-47-4
potassium tert-butylate

: 122270-83-1
{(R*,R*),(R*)}/{(R*,R*),(S*)}-(+/-)-(η5-cyclopentadienyl)(methylphenylphosphido){1,2-phenylenebis(methylphenylphosphine)}iron(II) monotetrahydrofuran solvate

Guidance literature:: In tetrahydrofuran; byproducts: KPF6; under Ar, stirring, 10 min; evapn. of solvent, extg. with toluene, filtration, evapn. of solvent in vac., dissolving in THF, pptg. by dilg. with n-hexane; elem. anal.;

Reference yield: 78.0%

: 113572-53-5
{(R*,R*),(S*)}-(+/-)-(η5-cyclopentadienyl)(methylphenylphosphine){1,2-phenylenebis(methylphenylphosphine)}iron(II) hexafluorophosphate monoacetone solvate

: 865-47-4
potassium tert-butylate

: 122270-83-1
{(R*,R*),(R*)}/{(R*,R*),(S*)}-(+/-)-(η5-cyclopentadienyl)(methylphenylphosphido){1,2-phenylenebis(methylphenylphosphine)}iron(II) monotetrahydrofuran solvate

Guidance literature:: In tetrahydrofuran; byproducts: KPF6; under Ar, stirring, 10 min; evapn. of solvent, extg. with toluene, filtration, evapn. of solvent in vac., dissolving in THF, pptg. by dilg. with n-hexane;