trans-bromo-(2,2-diphenylethylmercury)bis(triphenylphosphine)platinum

Base Information

Chemical Name:trans-bromo-(2,2-diphenylethylmercury)bis(triphenylphosphine)platinum
CAS No.:146245-42-3
Molecular Formula:C₅₀H₄₃BrHgP₂Pt
Molecular Weight:1181.41
Hs Code.:

Synonyms:

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Chemical Property of trans-bromo-(2,2-diphenylethylmercury)bis(triphenylphosphine)platinum

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Technology Process of trans-bromo-(2,2-diphenylethylmercury)bis(triphenylphosphine)platinum

There total 1 articles about trans-bromo-(2,2-diphenylethylmercury)bis(triphenylphosphine)platinum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 14221-02-4
tetrakis(triphenylphosphine)platinum

: 67341-84-8
1,1-diphenyl-2-(bromomercury)ethane

: 146245-42-3
trans-bromo-(2,2-diphenylethylmercury)bis(triphenylphosphine)platinum

Guidance literature:: In toluene; byproducts: P(C6H5)3; Ar, soln. of Pt-compound added to a soln. of Hg-compound, filtered; after 1 h hexane added, stored in darkness at 0°C for 24 h, filtered off, washed (hexane), dried in vacuo; elem. anal.;
DOI:10.1007/BF01558083

Reference yield: 70.0%

: 146245-42-3
trans-bromo-(2,2-diphenylethylmercury)bis(triphenylphosphine)platinum

: 99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0
fullerene-C₆₀

: 67341-84-8
1,1-diphenyl-2-(bromomercury)ethane

: C₆₀*Pt*2P(C₆H₅)3 = C₆₀Pt(P(C₆H₅)3)2

Guidance literature:: In dichloromethane; toluene; Ar, Pt-compound in CH2Cl2 mixed with C60, toluene added, stirred for 3 h (CH2Cl2 being removed from the reaction mixt. for 1 h); diluted with MeOH, stored for 5 days, C60-Pt-complex filtered off, washed (acetone, pentane), dried in vacuo, mother liquor and washouts combined, evapd., crystd. from EtOH gave the Hg-compound; elem. anal., NMR;
DOI:10.1007/BF01558083