chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(methylhexanoate)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolum bromide

Base Information

Chemical Name:chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(methylhexanoate)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolum bromide
CAS No.:1357287-34-3
Molecular Formula:Br*C₄₃H₅₄ClN₂O₄
Molecular Weight:778.27
Hs Code.:

chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(methylhexanoate)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolum bromide

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Chemical Property of chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(methylhexanoate)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolum bromide

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Technology Process of chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(methylhexanoate)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolum bromide

There total 2 articles about chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(methylhexanoate)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolum bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1-(5-carboxypentyl)-2,3,3-trimethylindoleninium bromide

: 63857-00-1,70446-42-3
N-[(3-(anilinomethylene)-2-chloro-1-cyclohexen-1-yl)methylene]aniline hydrochloride

: 1357287-34-3
chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(methylhexanoate)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolum bromide

: 1351459-84-1
chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(methylhexanoate)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(methylhexanoate)-3H-indolum bromide

: 172971-76-5
chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(5-carboxypentyl)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolum bromide

Guidance literature:: 1-(5-carboxypentyl)-2,3,3-trimethylindoleninium bromide; N-[(3-(anilinomethylene)-2-chloro-1-cyclohexen-1-yl)methylene]aniline hydrochloride; With sodium acetate; In acetic anhydride; at 90 ℃; for 3h; Inert atmosphere;

In methanol; for 0.166667h;
DOI:10.1016/j.bmcl.2011.11.070

Reference yield:

: 1640-39-7
2,3,3-trimethylindoleniune

: 1357287-34-3
chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(methylhexanoate)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolum bromide

: 1351459-84-1
chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(methylhexanoate)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(methylhexanoate)-3H-indolum bromide

: 172971-76-5
chloro-3-[2-[1,3-dihydro-3,3-dimethyl-1-(5-carboxypentyl)-2H-indol-2-ylidene]-ethylidene]-[[1-cyclo-1-yl]-ethenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolum bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetonitrile / 18 h / Inert atmosphere; Reflux

2.1: sodium acetate / acetic anhydride / 3 h / 90 °C / Inert atmosphere

2.2: 0.17 h

With sodium acetate; In acetic anhydride; acetonitrile;
DOI:10.1016/j.bmcl.2011.11.070