1.3-Bis-<4-(methyl-phenyl-carbamoyl)-phenyl>-harnstoff, 4,4'--carbanilid

Base Information

• Chemical Name: 1.3-Bis-<4-(methyl-phenyl-carbamoyl)-phenyl>-harnstoff, 4,4'--carbanilid
• CAS No.: 5100-33-4
• Molecular Formula: C₂₉H₂₆N₄O₃
• Molecular Weight: 478.55

Synonyms:

Chemical Property of 1.3-Bis-<4-(methyl-phenyl-carbamoyl)-phenyl>-harnstoff, 4,4'--carbanilid

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 1.3-Bis-<4-(methyl-phenyl-carbamoyl)-phenyl>-harnstoff, 4,4'--carbanilid

There total 3 articles about 1.3-Bis-<4-(methyl-phenyl-carbamoyl)-phenyl>-harnstoff, 4,4'--carbanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-isocyanatobenzoic acid chloride (3729-21-3) → 1.3-Bis-<4-(methyl-phenyl-carbamoyl)-phenyl>-harnstoff, 4,4'--carbanilid (5100-33-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / diethyl ether

2: H₂O

With water; triethylamine; In diethyl ether;

DOI:10.1021/jo01339a030

Reference yield:

p-aminobenzoic acid hydrochloride (22669-27-8) → 1.3-Bis-<4-(methyl-phenyl-carbamoyl)-phenyl>-harnstoff, 4,4'--carbanilid (5100-33-4)

Guidance literature:

Multi-step reaction with 3 steps

1: HCl / dioxane

2: Et₃N / diethyl ether

3: H₂O

With hydrogenchloride; water; triethylamine; In 1,4-dioxane; diethyl ether;

DOI:10.1021/jo01339a030

Reference yield:

N-Methyl-4-isocyanato-benzanilid (5100-27-6) → 1.3-Bis-<4-(methyl-phenyl-carbamoyl)-phenyl>-harnstoff, 4,4'--carbanilid (5100-33-4)

Guidance literature:

With water;

DOI:10.1021/jo01339a030

upstream raw materials:

N-Methyl-4-isocyanato-benzanilid

4-isocyanatobenzoic acid chloride

p-aminobenzoic acid hydrochloride

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