2-methyl-4-phenylpent-4-enoyl chloride

Base Information

Chemical Name:2-methyl-4-phenylpent-4-enoyl chloride
CAS No.:118451-42-6
Molecular Formula:C₁₂H₁₃ClO
Molecular Weight:208.688
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methyl-4-phenylpent-4-enoyl chloride

Chemical Property:

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Technology Process of 2-methyl-4-phenylpent-4-enoyl chloride

There total 3 articles about 2-methyl-4-phenylpent-4-enoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4432-63-7
2-phenylacrolein

: 118451-42-6
2-methyl-4-phenylpent-4-enoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / methanol / 2 h / Ambient temperature

2: 80 percent / hydroquinone / 3.5 h / 134 °C

3: 80 percent / aq. NaOH; ethanol

4: (COCl)2 / petroleum ether

With sodium tetrahydroborate; oxalyl dichloride; hydroquinone; In methanol; sodium hydroxide; ethanol; Petroleum ether;

Reference yield:

: 118451-39-1
ethyl 2-methyl-4-phenylpent-4-enoate

: 118451-42-6
2-methyl-4-phenylpent-4-enoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / aq. NaOH; ethanol

2: (COCl)2 / petroleum ether

With oxalyl dichloride; In sodium hydroxide; ethanol; Petroleum ether;

Reference yield:

: 98-83-9,6144-04-3,25014-31-7,42612-14-6
isopropenylbenzene

: 118451-42-6
2-methyl-4-phenylpent-4-enoyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1: t-BuOOH, SeO₂, salicylic acid / CH₂Cl₂ / 1) r.t., 2 h, 2) 25 deg C, 96 h

2: NaBH₄ / methanol / 2 h / Ambient temperature

3: 80 percent / hydroquinone / 3.5 h / 134 °C

4: 80 percent / aq. NaOH; ethanol

5: (COCl)2 / petroleum ether

With tert.-butylhydroperoxide; sodium tetrahydroborate; selenium(IV) oxide; oxalyl dichloride; hydroquinone; salicylic acid; In methanol; sodium hydroxide; ethanol; dichloromethane; Petroleum ether;