tris-{(pentafluoro phenyl) germyl} tris-{(pentafluoro phenyl) germyl mercury} sulfane

Base Information

Chemical Name:tris-{(pentafluoro phenyl) germyl} tris-{(pentafluoro phenyl) germyl mercury} sulfane
CAS No.:54666-70-5
Molecular Formula:C₃₆F₃₀Ge₂HgS
Molecular Weight:1380.18
Hs Code.:

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Chemical Property of tris-{(pentafluoro phenyl) germyl} tris-{(pentafluoro phenyl) germyl mercury} sulfane

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Technology Process of tris-{(pentafluoro phenyl) germyl} tris-{(pentafluoro phenyl) germyl mercury} sulfane

There total 2 articles about tris-{(pentafluoro phenyl) germyl} tris-{(pentafluoro phenyl) germyl mercury} sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 35406-49-6
bis[tris(pentafluorophenyl)germyl]mercury

: ((C₆F₅)3GeS)3Hg^(1-)*(C₅H₅)2Co⁽¹⁺⁾=((C₆F₅)3GeS)3Hg((C₅H₅)2Co)

: 54666-70-5
tris-{(pentafluoro phenyl) germyl} tris-{(pentafluoro phenyl) germyl mercury} sulfane

: (C₆F₅)3GeHg(SGe(C₆F₅)3)2^(1-)*(C₅H₅)2Co⁽¹⁺⁾=(C₆F₅)3GeHg(SGe(C₆F₅)3)2((C₅H₅)2Co)

Guidance literature:: In 1,2-dimethoxyethane; a DME soln. of (Ar3Ge)2Hg was added to a soln. of the trithiomercurate in DME, mixt. was kept in a sealed evacuated ampoule at 20°C for 1 h; solvent was evapd., residue extd. with hot hexane, ext. was cooled to give crystalline Ar3GeHgSHgAr3 (identified by LSC), insoluble in hexane residue was recrystd. from toluene-hexane yielding dithiomercurate complex (identified by IR spectrum);
DOI:10.1016/S0022-328X(00)99406-3