(η5-cyclopentadienyl)Pd(η1-cyclopentadienyl)PPh3

Base Information

Chemical Name:(η5-cyclopentadienyl)Pd(η1-cyclopentadienyl)PPh3
CAS No.:72244-79-2
Molecular Formula:C₂₈H₂₅PPd
Molecular Weight:498.9
Hs Code.:

Synonyms:

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Chemical Property of (η5-cyclopentadienyl)Pd(η1-cyclopentadienyl)PPh3

Chemical Property:

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Technology Process of (η5-cyclopentadienyl)Pd(η1-cyclopentadienyl)PPh3

There total 1 articles about (η5-cyclopentadienyl)Pd(η1-cyclopentadienyl)PPh3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72244-76-9
[Cl(PPh3)Pd]2(μ-OCOCH3)2

: 34822-90-7
cyclopentadienylthallium

: 72244-79-2
(η5-cyclopentadienyl)Pd(η1-cyclopentadienyl)PPh3

Guidance literature:: In toluene; under N2, soln. of Pd complex in toluene treated with TlC5H5, stirred at room temp. for 1-4 h; hexane added, filtered, allowed to stand at -78°C for several days, crystals filtered off, washed with cold pentane, dried in high vac.;elem. anal.;
DOI:10.1016/0022-328X(83)85075-X

Reference yield: 75.0%

: 72244-79-2
(η5-cyclopentadienyl)Pd(η1-cyclopentadienyl)PPh3

: 76-05-1
trifluoroacetic acid

: 87370-46-5
(η5-cyclopentadienyl)Pd(PPh3)OCOCF3

Guidance literature:: In pentane; under N2, suspn. of Pd complex in pentane cooled to -78°C, treated dropwise with vigorous stirring with soln. of CF3COOH in pentane, stirred for 2 h, warmed slowly to room temp.; decanted, residue dried in high vac., recrystd. from toluene/hexane; elem. anal.;
DOI:10.1016/0022-328X(83)85075-X

Reference yield:

: 72244-79-2
(η5-cyclopentadienyl)Pd(η1-cyclopentadienyl)PPh3

: (μ-cyclopentadienyl)2Pd2(PPh3)2

Guidance literature:: In hexane; toluene; under N2, soln. of educt in toluene treated with hexane, allowed to stand at room temp. for 5-7 days; NMR anal.;
DOI:10.1016/0022-328X(83)85075-X