methyl 4,7-di-O-acetyl-3,5-dideoxy-2-(4-methylphenylthio)-9-O-(methyl-4,7-di-O-acetyl-8,9-O-chloroacetyl-3,5-dideoxy-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosidonate

Base Information

• Chemical Name: methyl 4,7-di-O-acetyl-3,5-dideoxy-2-(4-methylphenylthio)-9-O-(methyl-4,7-di-O-acetyl-8,9-O-chloroacetyl-3,5-dideoxy-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosidonate
• CAS No.: 1172595-97-9
• Molecular Formula: C₄₃H₅₀Cl₂F₆N₂O₂₂S
• Molecular Weight: 1163.83
• Mol file: 1172595-97-9.mol

Synonyms:

Chemical Property of methyl 4,7-di-O-acetyl-3,5-dideoxy-2-(4-methylphenylthio)-9-O-(methyl-4,7-di-O-acetyl-8,9-O-chloroacetyl-3,5-dideoxy-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosidonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 4,7-di-O-acetyl-3,5-dideoxy-2-(4-methylphenylthio)-9-O-(methyl-4,7-di-O-acetyl-8,9-O-chloroacetyl-3,5-dideoxy-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosidonate

There total 1 articles about methyl 4,7-di-O-acetyl-3,5-dideoxy-2-(4-methylphenylthio)-9-O-(methyl-4,7-di-O-acetyl-8,9-O-chloroacetyl-3,5-dideoxy-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosidonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S,4S,5R,6R)-4-Acetoxy-6-((1R,2R)-1-acetoxy-2,3-dihydroxy-propyl)-2-p-tolylsulfanyl-5-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-carboxylic acid methyl ester (866332-36-7) + C34H37Cl2F3NO15P → methyl 4,7-di-O-acetyl-3,5-dideoxy-2-(4-methylphenylthio)-9-O-(methyl-4,7-di-O-acetyl-8,9-O-chloroacetyl-3,5-dideoxy-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosidonate (1172595-97-9) + methyl 4,7-di-O-acetyl-3,5-dideoxy-2-(4-methylphenylthio)-9-O-(methyl-4,7-di-O-acetyl-8,9-O-chloroacetyl-3,5-dideoxy-5-trifluoroacetamido-D-glycero-β-D-galacto-2-nonulopyranosylonate)-5-trifluoroacetamido-D-glycero-α-D-galacto-2-nonulopyranosidonate

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at -40 ℃; optical yield given as %de; Molecular sieve;

DOI:10.1016/j.tet.2009.04.022

upstream raw materials:

(2S,4S,5R,6R)-4-Acetoxy-6-((1R,2R)-1-acetoxy-2,3-dihydroxy-propyl)-2-p-tolylsulfanyl-5-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-2-carboxylic acid methyl ester