Co(propyl)(pyridine)(bis(phenylselanyl)glyoxime^(1-))2

Base Information

• Chemical Name: Co(propyl)(pyridine)(bis(phenylselanyl)glyoxime^(1-))2
• CAS No.: 1335030-59-5
• Molecular Formula: C₃₆H₃₄CoN₅O₄Se₄
• Molecular Weight: 975.53
• Mol file: 1335030-59-5.mol

Synonyms:

Chemical Property of Co(propyl)(pyridine)(bis(phenylselanyl)glyoxime^(1-))2

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Co(propyl)(pyridine)(bis(phenylselanyl)glyoxime^(1-))2

There total 1 articles about Co(propyl)(pyridine)(bis(phenylselanyl)glyoxime^(1-))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

Co(Cl)(pyridine)(bis(phenylselanyl)glyoxime(1-))2 (1335030-54-0) + propyl bromide (106-94-5) → Co(propyl)(pyridine)(bis(phenylselanyl)glyoxime(1-))2 (1335030-59-5)

Guidance literature:

With NaOH; NaBH₄; pyridine; In methanol; few drops of aq. NaOH added to Co-compd. in CH3OH, N2 gas bubbled through the solution with stirring for 20 min, pyridine added, aq. NaBH4 addedat 0°C, C3H7Br added, stirred at 0°C, slowly warmed to ro om temp., poured in ice cold H2O; filtered, washed with ice-cold H2O, dried, chromy. (silica gel, CH2Cl2),elem. anal.;

DOI:10.1016/j.jorganchem.2011.07.012

upstream raw materials:

Co(Cl)(pyridine)(bis(phenylselanyl)glyoxime^(1-))2

propyl bromide