Technology Process of C22H27N5O
There total 4 articles about C22H27N5O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethanol;
for 5h;
under 2068.65 Torr;
DOI:10.1002/asia.201000720
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; potassium iodide / acetonitrile / 12 h / Reflux; Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / ethanol / 5 h / 2068.65 Torr
With
palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium iodide;
In
ethanol; acetonitrile;
DOI:10.1002/asia.201000720
- Guidance literature:
-
Multi-step reaction with 3 steps
1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 20 °C
2: potassium carbonate; potassium iodide / acetonitrile / 12 h / Reflux; Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / ethanol / 5 h / 2068.65 Torr
With
carbon tetrabromide; palladium 10% on activated carbon; hydrogen; potassium carbonate; triphenylphosphine; potassium iodide;
In
tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1002/asia.201000720