(2E,4E)-Dodeca-2,4-dienoic acid [(1S,2R)-2-hydroxy-1-((E)-(5S,8S,10S)-10-methoxymethoxy-5-methyl-2,7-dioxo-1,6-diaza-cyclododec-3-en-8-ylcarbamoyl)-propyl]-amide

Base Information

• Chemical Name: (2E,4E)-Dodeca-2,4-dienoic acid [(1S,2R)-2-hydroxy-1-((E)-(5S,8S,10S)-10-methoxymethoxy-5-methyl-2,7-dioxo-1,6-diaza-cyclododec-3-en-8-ylcarbamoyl)-propyl]-amide
• CAS No.: 145958-14-1
• Molecular Formula: C₂₉H₄₈N₄O₇
• Molecular Weight: 564.723
• Mol file: 145958-14-1.mol

Synonyms:

Chemical Property of (2E,4E)-Dodeca-2,4-dienoic acid [(1S,2R)-2-hydroxy-1-((E)-(5S,8S,10S)-10-methoxymethoxy-5-methyl-2,7-dioxo-1,6-diaza-cyclododec-3-en-8-ylcarbamoyl)-propyl]-amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2E,4E)-Dodeca-2,4-dienoic acid [(1S,2R)-2-hydroxy-1-((E)-(5S,8S,10S)-10-methoxymethoxy-5-methyl-2,7-dioxo-1,6-diaza-cyclododec-3-en-8-ylcarbamoyl)-propyl]-amide

There total 1 articles about (2E,4E)-Dodeca-2,4-dienoic acid [(1S,2R)-2-hydroxy-1-((E)-(5S,8S,10S)-10-methoxymethoxy-5-methyl-2,7-dioxo-1,6-diaza-cyclododec-3-en-8-ylcarbamoyl)-propyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2(E),4(E)-dodecadienoic acid succinimido ester (145958-15-2) + (2S,3R)-2-Amino-3-hydroxy-N-((E)-(5S,8S,10S)-10-methoxymethoxy-5-methyl-2,7-dioxo-1,6-diaza-cyclododec-3-en-8-yl)-butyramide → glidobactin A (108351-50-4) + (2E,4E)-Dodeca-2,4-dienoic acid [(1S,2R)-2-hydroxy-1-((E)-(5S,8S,10S)-10-methoxymethoxy-5-methyl-2,7-dioxo-1,6-diaza-cyclododec-3-en-8-ylcarbamoyl)-propyl]-amide (145958-14-1)

Guidance literature:

With 4-methyl-morpholine; In N,N-dimethyl-formamide; for 24h; Yield given. Yields of byproduct given; Ambient temperature;

DOI:10.1039/c39920001687

Reference yield: 100.0%

(2E,4E)-Dodeca-2,4-dienoic acid [(1S,2R)-2-hydroxy-1-((E)-(5S,8S,10S)-10-methoxymethoxy-5-methyl-2,7-dioxo-1,6-diaza-cyclododec-3-en-8-ylcarbamoyl)-propyl]-amide (145958-14-1) → glidobactin A (108351-50-4)

Guidance literature:

With trifluoroacetic acid; In tetrahydrofuran; at 0 ℃; for 6h;

DOI:10.1039/c39920001687

upstream raw materials:

2(E),4(E)-dodecadienoic acid succinimido ester

Downstream raw materials:

glidobactin A