6-(carbobenzyloxyamino)caprioic imidazole

Base Information

Chemical Name:6-(carbobenzyloxyamino)caprioic imidazole
CAS No.:161012-51-7
Molecular Formula:C₁₇H₂₁N₃O₃
Molecular Weight:315.372
Hs Code.:

Synonyms:

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Chemical Property of 6-(carbobenzyloxyamino)caprioic imidazole

Chemical Property:

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Technology Process of 6-(carbobenzyloxyamino)caprioic imidazole

There total 1 articles about 6-(carbobenzyloxyamino)caprioic imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1947-00-8
6-(benzyloxycarbonylamino)hexanoic acid

: 530-62-1
1,1'-carbonyldiimidazole

: 161012-51-7
6-(carbobenzyloxyamino)caprioic imidazole

Guidance literature:: With dmap; In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1016/S0040-4039(00)78532-7

Reference yield:

: 16695-14-0
Malonic acid monomethyl ester

: 161012-51-7
6-(carbobenzyloxyamino)caprioic imidazole

: 152012-64-1
methyl 8-(benzyloxycarbonylamino)-3-oxooctanoate

Guidance literature:: Malonic acid monomethyl ester; With dibutylmagnesium; In tetrahydrofuran; n-heptane; at -78 - 20 ℃; for 1h;

6-(carbobenzyloxyamino)caprioic imidazole; In tetrahydrofuran; n-heptane; at 20 ℃; for 23h; Further stages.;
DOI:10.1021/jo016276m

Reference yield:

: 161012-51-7
6-(carbobenzyloxyamino)caprioic imidazole

: [5-(1-hydroxy-4-oxo-azetidin-2-yl)-pentyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: Bu₂Mg / tetrahydrofuran; heptane / 1 h / -78 - 20 °C

1.2: 6.626 g / tetrahydrofuran; heptane / 23 h / 20 °C

2.1: 95 percent / NaBH₄ / methanol / 0 °C

3.1: hydroxylamine hydrochloride; potassium hydroxide / methanol / 72 h

4.1: 1.905 g / CH₂Cl₂ / 19 h

5.1: 73 percent / triphenylphosphine; DBAD / acetonitrile / 4 h / 0 - 20 °C

6.1: potassium carbonate / methanol / 0.17 h / 0 - 5 °C

With potassium hydroxide; sodium tetrahydroborate; dibenzyl azodicarboxylate; dibutylmagnesium; hydroxylamine hydrochloride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; n-heptane; dichloromethane; acetonitrile; 1.2: Masamune-Brooks reaction / 5.1: Mitsunobu reaction;
DOI:10.1021/jo016276m