2-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-5a-carba-α-D-mannopyranose octa-N,O-acetate

Base Information

Chemical Name:2-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-5a-carba-α-D-mannopyranose octa-N,O-acetate
CAS No.:142967-90-6
Molecular Formula:C₂₉H₄₁NO₁₇
Molecular Weight:675.641
Hs Code.:

Synonyms:

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Chemical Property of 2-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-5a-carba-α-D-mannopyranose octa-N,O-acetate

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Technology Process of 2-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-5a-carba-α-D-mannopyranose octa-N,O-acetate

There total 6 articles about 2-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-5a-carba-α-D-mannopyranose octa-N,O-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142968-00-1
1,3-di-O-benzyl-4,6-O-benzylidene-5a-carba-α-D-mannopyranose

: 142967-90-6
2-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-5a-carba-α-D-mannopyranose octa-N,O-acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 62 percent / Hg(CN)2, Drierite / benzene / 72 h / Heating

2: H₂NNH₂*H₂O / 1.5 h / 100 °C

3: pyridine

4: H₂ / 20percent Pd(OH)2/C / ethanol / 760 Torr / Ambient temperature

5: pyridine

With pyridine; calcium sulfate; hydrogen; mercury(II) cyanide; hydrazine hydrate; palladium dihydroxide; In ethanol; benzene;
DOI:10.1016/S0008-6215(00)90484-1

Reference yield:

: Acetic acid (2R,3S,4R,5R,6S)-3-acetoxy-2-acetoxymethyl-5-amino-6-((4aR,6S,7R,8S,8aR)-6,8-bis-benzyloxy-2-phenyl-hexahydro-benzo[1,3]dioxin-7-yloxy)-tetrahydro-pyran-4-yl ester

: 142967-90-6
2-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-5a-carba-α-D-mannopyranose octa-N,O-acetate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: H₂ / 20percent Pd(OH)2/C / ethanol / 760 Torr / Ambient temperature

3: pyridine

With pyridine; hydrogen; palladium dihydroxide; In ethanol;
DOI:10.1016/S0008-6215(00)90484-1

Reference yield:

: 142968-02-3
1,3-di-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-mannopyranose

: 142967-90-6
2-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-5a-carba-α-D-mannopyranose octa-N,O-acetate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂NNH₂*H₂O / 1.5 h / 100 °C

2: pyridine

3: H₂ / 20percent Pd(OH)2/C / ethanol / 760 Torr / Ambient temperature

4: pyridine

With pyridine; hydrogen; hydrazine hydrate; palladium dihydroxide; In ethanol;
DOI:10.1016/S0008-6215(00)90484-1