C₂₃H₂₁NO₄Se

Base Information

Chemical Name:C₂₃H₂₁NO₄Se
CAS No.:1291090-01-1
Molecular Formula:C₂₃H₂₁NO₄Se
Molecular Weight:454.384
Hs Code.:

C<sub>23</sub>H<sub>21</sub>NO<sub>4</sub>Se

Synonyms:

Suppliers and Price of C₂₃H₂₁NO₄Se

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₂₁NO₄Se

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₂₁NO₄Se

There total 3 articles about C₂₃H₂₁NO₄Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (±)-ethyl 5-hydroxycyclohex-3-enecarboxylate

: 1291090-01-1
C₂₃H₂₁NO₄Se

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-methyl-1H-imidazole / tetrachloromethane / 18 h / 20 °C / Inert atmosphere

2.1: bis(η3-allyl-μ-chloropalladium(II)); caesium carbonate; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane / tetrahydrofuran / 0.25 h / 20 - 40 °C / Inert atmosphere

2.2: 20 h / 40 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

With 1-methyl-1H-imidazole; bis(η3-allyl-μ-chloropalladium(II)); caesium carbonate; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; lithium diisopropyl amide; In tetrahydrofuran; tetrachloromethane;
DOI:10.1002/chem.201003454

Reference yield:

: cis-ethyl 5-(tert-butoxycarbonyloxy)cyclohex-3-enecarboxylate

: 1291090-01-1
C₂₃H₂₁NO₄Se

Guidance literature:: Multi-step reaction with 2 steps

1.1: bis(η3-allyl-μ-chloropalladium(II)); caesium carbonate; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane / tetrahydrofuran / 0.25 h / 20 - 40 °C / Inert atmosphere

1.2: 20 h / 40 °C / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

With bis(η3-allyl-μ-chloropalladium(II)); caesium carbonate; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1002/chem.201003454

Reference yield:

: 10416-67-8
N-(trimethylsilyl)phthalimide

: 1291090-01-1
C₂₃H₂₁NO₄Se

Guidance literature:: Multi-step reaction with 2 steps

1.1: bis(η3-allyl-μ-chloropalladium(II)); (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane / tetrahydrofuran / 0.33 h / 40 °C / Inert atmosphere

1.2: 8 h / 40 °C / Inert atmosphere

1.3: 10 h / Inert atmosphere; Reflux

2.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

With bis(η3-allyl-μ-chloropalladium(II)); (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1002/chem.201003454