Technology Process of C21H20N4O4S2
There total 6 articles about C21H20N4O4S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide / ethanol; water / 1 h / 20 °C
2: hydrogen bromide / water / 36 h / Reflux
3: toluene-4-sulfonic acid / ethanol / Reflux
4: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide
5: water; lithium hydroxide
With
copper(l) iodide; water; hydrogen bromide; potassium carbonate; toluene-4-sulfonic acid; L-proline; sodium hydroxide; lithium hydroxide;
In
ethanol; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2012.01.047
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide / ethanol; water / 1 h / 20 °C
2: hydrogen bromide / water / 36 h / Reflux
3: toluene-4-sulfonic acid / ethanol / Reflux
4: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide
5: water; lithium hydroxide
With
copper(l) iodide; water; hydrogen bromide; potassium carbonate; toluene-4-sulfonic acid; L-proline; sodium hydroxide; lithium hydroxide;
In
ethanol; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2012.01.047
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen bromide / water / 36 h / Reflux
2: toluene-4-sulfonic acid / ethanol / Reflux
3: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide
4: water; lithium hydroxide
With
copper(l) iodide; water; hydrogen bromide; potassium carbonate; toluene-4-sulfonic acid; L-proline; lithium hydroxide;
In
ethanol; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2012.01.047