2-chloro-4-nitro-phenyl thiocyanate

Base Information

• Chemical Name: 2-chloro-4-nitro-phenyl thiocyanate
• CAS No.: 408350-99-2
• Molecular Formula: C₇H₃ClN₂O₂S
• Molecular Weight: 214.632
• Mol file: 408350-99-2.mol

Synonyms:

Chemical Property of 2-chloro-4-nitro-phenyl thiocyanate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-chloro-4-nitro-phenyl thiocyanate

There total 3 articles about 2-chloro-4-nitro-phenyl thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloro-2-thiocyanatobenzene (2457-37-6) → 2-chloro-4-nitro-phenyl thiocyanate (408350-99-2) + 2-chloro-5-nitrophenyl thiocyanate (89880-52-4)

Guidance literature:

With nitric acid; at -6 ℃;

DOI:10.1039/jr9300000026

Reference yield:

2-Chloro-4-nitroaniline (121-87-9) → 2-chloro-4-nitro-phenyl thiocyanate (408350-99-2)

Guidance literature:

With sulfuric acid; Diazotization_.Behandlung der Diazoniumsalz-Loesung mit Kaliumthiocyanat und FeCl₃;

DOI:10.1039/jr9300000026

Reference yield:

N-(2-chloro-4-nitrophenyl)acetamide (881-87-8) → 2-chloro-4-nitro-phenyl thiocyanate (408350-99-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous sulfuric acid

2: aqueous H₂SO₄ / Diazotization_.Behandlung der Diazoniumsalz-Loesung mit Kaliumthiocyanat und FeCl₃

With sulfuric acid;

DOI:10.1039/jr9300000026

upstream raw materials:

1-chloro-2-thiocyanatobenzene

2-Chloro-4-nitroaniline

N-(2-chloro-4-nitrophenyl)acetamide

Downstream raw materials:

2-chloro-1-(methylsulfanyl)-4-nitrobenzene

2-Chloro-1-ethylsulfanyl-4-nitro-benzene

2-chloro-4-nitrophenyl methyl sulfone

1,2-bis(2-chloro-4-nitrophenyl)disulfane