3α-(N-Carbethoxy)amino-1αH,5αH-nortropane

Base Information

Chemical Name:3α-(N-Carbethoxy)amino-1αH,5αH-nortropane
CAS No.:83791-18-8
Molecular Formula:C₁₀H₁₈N₂O₂
Molecular Weight:198.265
Hs Code.:

Synonyms:

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Chemical Property of 3α-(N-Carbethoxy)amino-1αH,5αH-nortropane

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Technology Process of 3α-(N-Carbethoxy)amino-1αH,5αH-nortropane

There total 4 articles about 3α-(N-Carbethoxy)amino-1αH,5αH-nortropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83791-15-5
8-Benzyl-3α-(N-carbethoxy)amino-1αH,5αH-nortropane

: 83791-18-8
3α-(N-Carbethoxy)amino-1αH,5αH-nortropane

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; for 24h; under 1802 Torr; Ambient temperature;
DOI:10.1002/jhet.5570190307

Reference yield:

: 76272-35-0
3 α-amino-8-phenylmethyl-8-azabicyclo<3,2,1>octane

: 83791-18-8
3α-(N-Carbethoxy)amino-1αH,5αH-nortropane

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / Anhydrous sodium carbonate / acetonitrile / 1.) 0 deg C, 2.) reflux, 16 h

2: Hydrogen, Acetic acid / 10percent Palladium-on-carbon / ethanol / 24 h / 1802 Torr / Ambient temperature

With hydrogen; sodium carbonate; acetic acid; palladium on activated charcoal; In ethanol; acetonitrile;
DOI:10.1002/jhet.5570190307

Reference yield:

: 28957-72-4
N-benzylnortropinone

: 83791-18-8
3α-(N-Carbethoxy)amino-1αH,5αH-nortropane

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / Hydroxylamine hydrochloride, sodium bicarbonate / aq. ethanol / 0.5 h / 100 °C

2: 46 percent / Hydrogen / Platinum oxide / ethanol; acetic acid / 48 h / 2316.8 Torr

3: 81 percent / Anhydrous sodium carbonate / acetonitrile / 1.) 0 deg C, 2.) reflux, 16 h

4: Hydrogen, Acetic acid / 10percent Palladium-on-carbon / ethanol / 24 h / 1802 Torr / Ambient temperature

With hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; sodium carbonate; acetic acid; platinum(IV) oxide; palladium on activated charcoal; In ethanol; acetic acid; acetonitrile;
DOI:10.1002/jhet.5570190307