3-phenyl-4-(4-methylphenyl)-1-(phenylsulfonyl)-β-carbonline

Base Information

Chemical Name:3-phenyl-4-(4-methylphenyl)-1-(phenylsulfonyl)-β-carbonline
CAS No.:1391983-93-9
Molecular Formula:C₃₀H₂₂N₂O₂S
Molecular Weight:474.583
Hs Code.:

Synonyms:

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Chemical Property of 3-phenyl-4-(4-methylphenyl)-1-(phenylsulfonyl)-β-carbonline

Chemical Property:

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Technology Process of 3-phenyl-4-(4-methylphenyl)-1-(phenylsulfonyl)-β-carbonline

There total 7 articles about 3-phenyl-4-(4-methylphenyl)-1-(phenylsulfonyl)-β-carbonline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1391983-91-7
4-iodine-3-phenyl-1-(phenylsulfonyl)-β-carbonline

: 5720-05-8
4-methylphenylboronic acid

: 1391983-93-9
3-phenyl-4-(4-methylphenyl)-1-(phenylsulfonyl)-β-carbonline

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; In toluene; at 45 - 60 ℃; for 20h;
DOI:10.1016/j.cclet.2012.09.010

Reference yield:

: 95-20-5
2-methyl-1H-indole

: 1391983-93-9
3-phenyl-4-(4-methylphenyl)-1-(phenylsulfonyl)-β-carbonline

Guidance literature:: Multi-step reaction with 7 steps

1: iodine; potassium hydroxide / N,N-dimethyl-formamide / 4 h / 20 °C

2: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / water; benzene / 12 h / 20 °C

3: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 35 °C / Inert atmosphere

4: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux

5: sodium azide; tetra(n-butyl)ammonium hydrogensulfate / water; Petroleum ether / 12 h / Reflux

6: iodine / nitromethane / 20 h / 105 °C

7: bis-triphenylphosphine-palladium(II) chloride; potassium phosphate / toluene / 20 h / 45 - 60 °C

With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; N-Bromosuccinimide; copper(l) iodide; sodium azide; 2,2'-azobis(isobutyronitrile); iodine; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; potassium hydroxide; sodium hydroxide; In tetrachloromethane; nitromethane; water; N,N-dimethyl-formamide; toluene; Petroleum ether; benzene;
DOI:10.1016/j.cclet.2012.09.010

Reference yield:

: 2033-44-5
3-iodoindole-2-methylindole

: 1391983-93-9
3-phenyl-4-(4-methylphenyl)-1-(phenylsulfonyl)-β-carbonline

Guidance literature:: Multi-step reaction with 6 steps

1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / water; benzene / 12 h / 20 °C

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 35 °C / Inert atmosphere

3: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux

4: sodium azide; tetra(n-butyl)ammonium hydrogensulfate / water; Petroleum ether / 12 h / Reflux

5: iodine / nitromethane / 20 h / 105 °C

6: bis-triphenylphosphine-palladium(II) chloride; potassium phosphate / toluene / 20 h / 45 - 60 °C

With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; N-Bromosuccinimide; copper(l) iodide; sodium azide; 2,2'-azobis(isobutyronitrile); iodine; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; sodium hydroxide; In tetrachloromethane; nitromethane; water; toluene; Petroleum ether; benzene;
DOI:10.1016/j.cclet.2012.09.010