Na(acacPhF₃)

Base Information

• Chemical Name: Na(acacPhF₃)
• CAS No.: 19269-15-9
• Molecular Formula: C₁₀H₆F₃O₂*Na
• Molecular Weight: 238.141

Synonyms:

Chemical Property of Na(acacPhF₃)

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Na(acacPhF₃)

There total 1 articles about Na(acacPhF₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,1-trifluoro-4-hydroxy-4-phenyl-but-3-en-2-one (66929-54-2) → Na(acacPhF3) (19269-15-9)

Guidance literature:

With sodium; In 1,4-dioxane; at 20 ℃;

DOI:10.1134/S0022476612040178

Reference yield: 25.0%

potassium hydridotris(3,5-diphenylpyrazol-1-yl)borate + Na(acacPhF3) (19269-15-9) + iron(II) chloride → [Fe(Ph2Tp)(acacPhF3)] (1346159-75-8)

Guidance literature:

In acetonitrile; byproducts: NaCl, KCl; (inert atm.); addn. of iron compd., borate deriv. and CH3CN to sodium acetylacetonate deriv., stirring overnight at room temp.; evapn., dissolving in CH2Cl2, filtration, layering with CH3CN, isolationof crystals, elem. anal.;

DOI:10.1021/ic201115s

Reference yield:

iron(II) triflate + tris(2-phenyl-1H-imidazol-5-yl)phosphane (1023795-23-4) + Na(acacPhF3) (19269-15-9) → [Fe(PhTIP)(acacPhF3)](triflate)

Guidance literature:

In methanol; (inert atm.); addn. of methanolic soln. of iron compd. and phosphine deriv. to methanolic soln. of sodium acetylacetonate deriv., stirring overnight at room temp.; evapn., dissolving in CH2Cl2, filtration, layering with pentane, isolation of crystals, elem. anal.;

DOI:10.1021/ic201115s

upstream raw materials:

1,1,1-trifluoro-4-hydroxy-4-phenyl-but-3-en-2-one

Downstream raw materials:

[Fe(Ph₂Tp)(acacPhF₃)]

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